3',5'-二氯-2'-羟基苯乙酮合成路线 （共 15 条）
反应条件
aluminium trichloride T=135°C;
参考文献
Journal of the Indian Chemical Society, , vol. 26, p. 366,367
Journal of the American Chemical Society, , vol. 64, p. 607,611
Journal of the Chinese Chemical Society (Peking), , vol. 7, p. 40
Chem.Abstr., , p. 1979
反应条件
chlorine; iron(III) chloride in water
反应条件
aluminium trichloride T=180°C; 0.5 h;
参考文献
Kim, Jae Nyoung; Ryu, Eung K.
Synthetic Communications, 1996 , vol. 26, # 1 p. 67 - 74
反应条件
sodium perborate in acetic acid deoximation; 5.5 h; Heating;
参考文献
Jadhav, Vidyadhar K.; Deshmukh, Anjali P.; Wadagaonkar, Prakash P.; Salunkhe, Manikrao M.
Synthetic Communications, 2000 , vol. 30, # 8 p. 1521 - 1527
反应条件
sodium acetate; chlorine; acetic acid T=20°C; 0.5 h;
参考文献
Rajput, P. R.; Gajbhiye, A. V.; Bhade, M. W.
Asian Journal of Chemistry, 2012 , vol. 24, # 12 p. 5699 - 5701,3
Title/Abstract Full Text Show Details
Rajput; Gajbhiye; Bhade
Asian Journal of Chemistry, 2012 , vol. 24, # 12 p. 5699 - 5701
反应条件
1: pyridine 2: AlCl3 / 135 °C View Scheme
参考文献
Journal of the American Chemical Society, , vol. 64, p. 607,611
反应条件
2,2,6,6-tetramethyl-piperidine; sulfuryl dichloride T=100°C; 0.75 h; Inert atmosphere; regioselective reaction;
参考文献
Saper, Noam I.; Snider, Barry B.
Journal of Organic Chemistry, 2014 , vol. 79, # 2 p. 809 - 813
反应条件
N-chloro-succinimide T=80°C; 10 h; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 77, # 13 p. 5823 - 5828
参考文献
Journal of the American Chemical Society, , vol. 64, p. 607,611
Journal of the Chinese Chemical Society (Peking), , vol. 7, p. 40
Chem.Abstr., , p. 1979
反应条件
1: N,N-dimethyl-formamide With bis(trichloromethyl) carbonate in 1,2-dichloro-ethane T=0 - 20°C; 2: 3',5'-dichloro-2'-hydroxyacetophenone in 1,2-dichloro-ethane T=0 - 20°C; 4.5 h; Further stages.;
参考文献
Su; Li; Zhao
Organic Preparations and Procedures International, 2007 , vol. 39, # 5 p. 495 - 502
