2-甲基-2,3-二氢-1H-茚-2-醇合成路线 （共 14 条）
反应条件
1: methyllithium With titanium tetrachloride in diethyl ether T=-80°C; 0.25 h; 2: indan-2-one in diethyl ether T=-50 - 20°C; 3: With water in diethyl ether
参考文献
Doherty, Elizabeth M.; Katon, Jodie; Norman, Mark H.; Retz, Daniel M.; Wang, Xianghong; Bo, Yunxin Y.; Tamayo, Nuria; Nishimura, Nobuko; Liao, Hongyu
Patent: US2006/241296 A1, 2006 ;
Location in patent: Page/Page column 63 ;
US 20060241296 A1
反应条件
methylmagnesium bromide; ammonium chloride; sodium hydrogencarbonate in diethyl ether; hexane; water
参考文献
Moore, Jennifer L.; Kerr, Mark S.; Rovis, Tomislav
Tetrahedron, 2006 , vol. 62, # 49 p. 11477 - 11482
反应条件
in diethyl ether T=0°C; 3 h;
参考文献
Reetz, M. T.; Kyung, S. H.; Huellmann, M.
Tetrahedron, 1986 , vol. 42, # 11 p. 2931 - 2935
反应条件
magnesium Grignard reaction;
参考文献
Bowers, Nigel I.; Boyd, Derek R.; Sharma, Narain D.; Goodrich, Peter A.; Groocock, Melanie R.; Blacker, A. John; Goode, Paul; Dalton, Howard
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 11 p. 1453 - 1461
参考文献
Wilt,J.W. et al.
Journal of Organic Chemistry, 1972 , vol. 37, # 6 p. 820 - 825
反应条件
in diethyl ether Heating;
参考文献
Hamza, Abdulhamid
Structural Chemistry, 2010 , vol. 21, # 5 p. 939 - 945
反应条件
potassium dichromate; potassium carbonate in benzene Ambient temperatureIrradiationother ketones, sensitization with tetramethyl-1,2-dioxetane; other temp., other solvent; Product distribution;
参考文献
Noh, Taehee; Lei, Xue-Gong; Turro, Nicholas J.
Journal of the American Chemical Society, 1993 , vol. 115, # 8 p. 3105 - 3110
反应条件
toluene-4-sulfonic acid in benzene Dehydration; 4 h; Heating;
参考文献
Bowers, Nigel I.; Boyd, Derek R.; Sharma, Narain D.; Goodrich, Peter A.; Groocock, Melanie R.; Blacker, A. John; Goode, Paul; Dalton, Howard
Journal of the Chemical Society - Perkin Transactions 1, 1999 , # 11 p. 1453 - 1461
反应条件
MeMgBr; toluene-4-sulfonic acid; hydroquinone in toluene
参考文献
Exxon Chemical Patents Inc.
Patent: US5541350 A1, 1996 ;
参考文献
Koelsch; Johnson
Journal of the American Chemical Society, 1943 , vol. 65, p. 565
