4,6-二-O-乙酰基-2,3-二脱氧-Alpha-D-赤式-六-2-烯桥吡喃糖苷乙酯合成路线 (共 15 条)
反应条件
iodine in dichloromethane
参考文献
Tetrahedron Letters, , vol. 44, # 33 p. 6211 - 6215
反应条件
ethanol; ammonium chloride
参考文献
Journal of the Chemical Society, , p. 738,742
Justus Liebigs Annalen der Chemie, , vol. 443, p. 223,237
反应条件
1: 2.2 g / H2 / Pd/C / ethanol / 20 °C 2: 1.22 g / MeONa / methanol / 1.5 h / 25 °C View Scheme
参考文献
Mishra, Shri Krishna; Rao, R Balaji
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1993 , vol. 32, # 5 p. 562 - 563
反应条件
aluminium trichloride in dichloromethane
0.75 h; 1.) -45 deg C, 2.) 0 deg C; Yields of byproduct given;
参考文献
Dawe, Robert David; Fraser-Reid, Bert
Journal of Organic Chemistry, 1984 , vol. 49, # 3 p. 522 - 528
反应条件
in chloroform
T=4°C; 96 h;
参考文献
Gnichtel, Horst; Autenrieth, Leonore; Luger, Peter; Vangehr, Kristina
Liebigs Annalen der Chemie, 1982 , # 6 p. 1091 - 1095