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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
33240-33-4
合成路线
（共 10 条）
507-20-0
氯代叔丁烷
+
85-01-8
菲
→
反应条件
33240-33-4
+
66553-04-6
反应条件
aluminium trichloride in tetrachloromethane; nitromethane T=40 - 45°C; 3 h;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
507-20-0
氯代叔丁烷
+
85-01-8
菲
→
反应条件
33240-33-4
+
64392-49-0
+
66553-04-6
+
119561-11-4
+
24300-92-3
反应条件
aluminium trichloride in nitromethane T=20°C; 0.5 h; other molar ratio, other time, other catalyst; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
78-83-1
异丁醇
+
85-01-8
菲
→
反应条件
33240-33-4
+
66553-04-6
反应条件
cyclohexane; boron trifluoride; phosphorus pentoxide
参考文献
Imagire
Kogyo Kagaku Zasshi, 1959 , vol. 62, p. 837,839
Chem.Abstr., 1962 , vol. 57, p. 8517
85-01-8
菲
+
75-65-0
叔丁醇
→
反应条件
33240-33-4
+
66553-04-6
反应条件
cyclohexane; boron trifluoride; phosphorus pentoxide
参考文献
Imagire
Kogyo Kagaku Zasshi, 1959 , vol. 62, p. 837,839
Chem.Abstr., 1962 , vol. 57, p. 8517
66553-04-6
→
反应条件
85-01-8
菲
+
33240-33-4
+
64392-49-0
+
119561-11-4
+
24300-92-3
反应条件
aluminium trichloride in tetrachloromethane; nitromethane T=40°C; 5 h; other reaction time; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
64392-49-0
→
反应条件
85-01-8
菲
+
33240-33-4
+
66553-04-6
+
119561-11-4
+
24300-92-3
反应条件
aluminium trichloride in tetrachloromethane; nitromethane T=40°C; 3.5 h; other reaction time; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
119561-11-4
→
反应条件
85-01-8
菲
+
33240-33-4
+
64392-49-0
+
66553-04-6
+
24300-92-3
反应条件
aluminium trichloride in tetrachloromethane; nitromethane T=40°C; 7 h; other reaction time; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
24300-92-3
→
反应条件
85-01-8
菲
+
33240-33-4
+
64392-49-0
+
66553-04-6
+
119561-11-4
反应条件
aluminium trichloride in tetrachloromethane; nitromethane T=40°C; 6 h; other reaction time; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
20374-76-9
→
反应条件
33240-33-4
反应条件
(UV-irradiation);
参考文献
Cameron,D.W.; Mingin,M.
Australian Journal of Chemistry, 1977 , vol. 30, p. 859 - 863
85-01-8
菲
+
75-65-0
叔丁醇
→
反应条件
33240-33-4
+
64392-49-0
+
66553-04-6
+
119561-11-4
+
24300-92-3
反应条件
trifluoroacetic acid 6 h; Heatingother molar ratio, other time; Product distribution;
参考文献
Pozdnyakovich, Yu. A.
Journal of Organic Chemistry USSR (English Translation), 1988 , vol. 24, # 5 p. 972 - 977
Zhurnal Organicheskoi Khimii, 1988 , vol. 24, # 5 p. 1076 - 1082
