oxalyl dichloride; dimethyl sulfoxide; triethylamine in dichloromethane T=-60°C; 0.25 h;
参考文献
Barton, Derek H. R.; Boivin, Jean; Gastiger, Michel; Morzycki, Jacek; Hay-Motherwell, Robyn S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 947 - 956
oxygen; acetic acid; zinc; lt;Fe3O(O2CCH3)6(C5H5N)3gt;2C5H5N in pyridine; water T=20°C; 4 h; Title compound not separated from byproducts;
参考文献
Barton, Derek H. R.; Boivin, Jean; Gastiger, Michel; Morzycki, Jacek; Hay-Motherwell, Robyn S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 947 - 956
1: 61 percent / pyridine / 36 h / 20 °C 2: 52 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating 3: 78 percent / oxalyl chloride, Me2SO, Et3N / CH2Cl2 / 0.25 h / -60 °C View Scheme
参考文献
Barton, Derek H. R.; Boivin, Jean; Gastiger, Michel; Morzycki, Jacek; Hay-Motherwell, Robyn S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 947 - 956
1: 52 percent / LiAlH4 / tetrahydrofuran / 4 h / Heating 2: 78 percent / oxalyl chloride, Me2SO, Et3N / CH2Cl2 / 0.25 h / -60 °C View Scheme
参考文献
Barton, Derek H. R.; Boivin, Jean; Gastiger, Michel; Morzycki, Jacek; Hay-Motherwell, Robyn S.; et al.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1986 , p. 947 - 956
