3,6-二溴-9-乙基咔唑合成路线 （共 17 条）
反应条件
N-bromosuccinmide in dichloromethane T=25°C;
参考文献
Samsung Electronics Co., Ltd.; Yang, Hye-yeon; Joo, Won-jae; Son, Jhun-mo; Kang, Ho-suk
Patent: US8558007 B2, 2013 ;
Location in patent: Page/Page column 28; 29 ;
反应条件
potassium hydroxide in dimethyl sulfoxide T=50°C; 24 h; Inert atmosphere;
参考文献
Shen, Ping; Tang, Yuhua; Jiang, Shenghui; Chen, Huajie; Zheng, Xiaoyan; Wang, Xueye; Zhao, Bin; Tan, Songting
Organic Electronics: physics, materials, applications, 2011 , vol. 12, # 1 p. 125 - 135
反应条件
KBrO3; hydrogenchloride; acetic acid; potassium bromide
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 66, p. 533,541
反应条件
1: acetone; aqueous KOH-solution 2: tetrachloromethane; N-bromo-succinimide View Scheme
参考文献
Recueil des Travaux Chimiques des Pays-Bas, , vol. 66, p. 533,541
反应条件
potassium hydroxide; acetone
参考文献
Journal of the American Chemical Society, , vol. 63, p. 1553,1554
反应条件
N-bromosuccinmide; silica gel in dichloromethane T=18°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Tetrahedron, , vol. 48, # 36 p. 7479 - 7488
反应条件
bromine; acetic acid 0.333333 h; Ambient temperature;
参考文献
Tetrahedron, , vol. 54, # 42 p. 12707 - 12714
反应条件
bromine; acetic acid
参考文献
DE700554 , ;
DRP/DRBP Org.Chem.
参考文献
Diss., <Braunschweig 1926>25
反应条件
n-butyllithium; diethyl ether; benzene anschliessendes Behandeln mit festem CO2;
参考文献
Gilman; Spatz
Journal of the American Chemical Society, 1941 , vol. 63, p. 1553,1554
