2'-羟基-2-(4-甲氧基亚苄基)乙酰苯合成路线 (共 22 条)
反应条件
1: 80 percent / copper(II) chloride-DMSO / 2 h / Heating 2: 60 percent / 10percent KOH / ethanol / 2 h / Heating View Scheme
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
反应条件
1-methylimidazolium nitrate T=80°C; 2 h; Inert atmosphereGreen chemistry;
参考文献
Loghmani-Khouzani, Hossein; Tamjidi, Panteha; Mohammadpoor-Baltork, Iraj; Yaeghoobi, Marzieh; Rahman, Noorsaadah Abd.; Khosropour, Ahmad Reza; Moghadam, Majid; Tangestaninejad, Shahram; Mirkhani, Valiolah; Habibi, Mohammad Hossein; Kashima, Ayana; Suzuki, Takayoshi
Journal of Heterocyclic Chemistry, 2014 , vol. 51, # 1 p. 138 - 150
反应条件
1: 80 percent / acid-catalyzed cyclization
2: 59 percent / thallium trinitrate, 70percent perchloric acid / CHCl3; methanol / 25 °C
View Scheme
参考文献
Kinoshita, Takeshi; Ichinose, Koji; Sankawa, Ushio
Tetrahedron Letters, 1990 , vol. 31, # 50 p. 7355 - 7356
反应条件
copper(II) chloride-DMSO
2 h; Heating;
参考文献
Sahasrabhuddhe; Ghiya
Indian Journal of Chemistry - Section B Organic Chemistry Including Medicinal Chemistry, 1990 , vol. 29, # 1 p. 61 - 63
反应条件
1: sodium tetrahydroborate / isopropyl alcohol
2: (tetraoctylammonium)AuCl4; water / dichloromethane / 24 h / 20 °C
View Scheme
参考文献
Maiti, Gourhari; Kayal, Utpal; Karmakar, Rajiv; Bhattacharya, Rudraksha N.
Tetrahedron Letters, 2012 , vol. 53, # 47 p. 6321 - 6325,5
反应条件
1: 90.94 percent / alkaline H2O2
2: 78 percent / K2CO3 / acetone
View Scheme
参考文献
Dhoubhadel, S. P.; Tuladhar, Sudersan M.; Tuladhar, Sarbajna M.; Wagley, Pradyumna P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1981 , vol. 20, # 6 p. 511 - 512
反应条件
silica ferric hydrogensulphate in ethanol
Michael Addition; 9 h; Reflux;
参考文献
Eshghi, Hossein; Rahimizadeh, Mohammad; Mousavi, Seyed Mohsen
Natural Product Research, 2014 , vol. 28, # 7 p. 438 - 443
反应条件
iodine; acetic acid in ethanol; water
Reflux;
参考文献
Sagrera, Gabriel; Bertucci, Ana; Vazquez, Alvaro; Seoane, Gustavo
Bioorganic and Medicinal Chemistry, 2011 , vol. 19, # 10 p. 3060 - 3073
反应条件
pyridine; hydroxylamine hydrochloride in ethanol
6 h; Heating;
参考文献
Witczak, Zbigniew; Krolikowska, Maria
Polish Journal of Chemistry, 1981 , vol. 55, # 1 p. 89 - 100
反应条件
potassium hydroxide; hydroxylamine hydrochloride in ethanol
参考文献
Witczak, Zbigniew; Krolikowska, Maria
Polish Journal of Chemistry, 1981 , vol. 55, # 4 p. 763 - 773