戊-3-炔基 4-甲基苯磺酸酯合成路线 （共 17 条）
反应条件
4-(N,N-dimethlyamino)pyridine; triethylamine Inert atmosphere;
参考文献
Fang, Fang; Vogel, Megan; Hines, Jennifer V.; Bergmeier, Stephen C.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 15 p. 3080 - 3091
反应条件
1: Na2CO3 / various solvent(s) / 24 h / 80 °C 2: 69 percent / pyridine / 1.) 1 h, room temp., 2.) 24 h, refrigerator View Scheme
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
1: NaI / acetone 2: Mg / diethyl ether View Scheme
参考文献
Ansell,M.F. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 217 - 225
反应条件
diethylene glycol monoethyl ether; CaBr2
参考文献
Flahaut,J.; Miginiac,P.
Helvetica Chimica Acta, 1978 , vol. 61, p. 2275 - 2285
反应条件
sodium carbonate in various solvent(s) T=50°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate in various solvent(s) T=50°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate in various solvent(s)
T=25°C; 720 h;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
trifluoroacetic acid sodium salt in trifluoroacetic acid
T=50°C; 264 h;
参考文献
Hanack,M. et al.
Justus Liebigs Annalen der Chemie, 1970 , vol. 733, p. 5 - 26
反应条件
sodium carbonate
T=80°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
1: (alkaline hydrolysis)
2: (i) (irradiation), tBuOCl, (ii) Na2CO3
View Scheme
参考文献
Poutsma,M.L.; Ibarbia,P.A.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4038 - 4047
