戊-3-炔基 4-甲基苯磺酸酯合成路线 （共 17 条）
反应条件
1: NaOEt / ethanol
2: aq. KOH / ethanol
3: 2 h / 150 °C
4: LiAlH4 / diethyl ether
View Scheme
参考文献
Ansell,M.F. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 217 - 225
反应条件
sodium carbonate in various solvent(s)
T=25°C; 720 h;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate in various solvent(s)
T=50°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate in various solvent(s)
T=50°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
sodium carbonate
T=80°C; 720 h; Further byproducts given;
参考文献
Collins, Clair J.; Hanack, Michael; Stutz, Herbert; Auchter, Gerhard; Schoberth, Winfried
Journal of Organic Chemistry, 1983 , vol. 48, # 26 p. 5260 - 5268
反应条件
(alkaline hydrolysis);
参考文献
Poutsma,M.L.; Ibarbia,P.A.
Journal of Organic Chemistry, 1970 , vol. 35, p. 4038 - 4047
反应条件
1: NaI / acetone
2: (i) Mg, Et2O, (ii) /BRN= 1900390/
View Scheme
参考文献
Ansell,M.F. et al.
Journal of the Chemical Society [Section] C: Organic, 1968 , p. 217 - 225
