in water addn. of 90g KSCN in 840ml H2O to 150g Pb(NO3)2 in 1500ml H2O at ambient temp. while stirring, cooling, crystn.;; filtration in the cold, washing with ice-cooled H2O, drying on clay in the dark; yield: 90g;;
Hall
Journal of the American Chemical Society, vol. 24, p. 570
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Boettger
Zeitschrift fuer Physikalische Chemie, Stoechiometrie und Verwandtschaftslehre, vol. 46, p. 576