2H-全氟(5-甲基-3,6-二氧杂壬烷)合成路线 (共 11 条)
反应条件
potassium fluoride in acetonitrile T=70°C; 4 h; Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride; bromine in acetonitrile T=75°C; 10 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
iodine; potassium carbonate in N,N-dimethyl-formamide Heating;
参考文献
Russian Journal of General Chemistry, , vol. 81, # 9 p. 1829 - 1833
反应条件
tetrakis(triphenylphosphine) palladium(0) T=95°C; 4 h;
参考文献
Journal of Fluorine Chemistry, , vol. 42, p. 355 - 370
反应条件
tetrakis(triphenylphosphine) palladium(0); n-pentylcarbonyl chloride T=95°C; 4 h;
参考文献
Journal of Fluorine Chemistry, , vol. 42, p. 355 - 370
反应条件
potassium fluoride in acetonitrile T=75°C; 20 h; Further byproducts given. Yields of byproduct given;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
potassium fluoride in acetonitrile T=70°C; 16 h;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
cesium fluoride in diethyl ether T=0°C; 3 h; Further byproducts given;
参考文献
Journal of Fluorine Chemistry, , vol. 69, # 1 p. 61 - 66
反应条件
potassium fluoride in acetonitrile also with CsF; also with Br2 and further substrates; Product distributionMechanism;
参考文献
Journal of Fluorine Chemistry, , vol. 55, # 1 p. 93 - 100
反应条件
sodium hydroxide Heating; Yield given;
参考文献
Journal of Fluorine Chemistry, , vol. 80, # 2 p. 125 - 134