9,10-二氢苯并(A)芘-7(8H)-酮合成路线 (共 24 条)
反应条件
toluene-4-sulfonic acid; 3-hydroxy-2,2-dimethylpropanol in toluene 8 h; Reflux;
参考文献
Imai, Masao; Morais, Goreti Ribeiro; Al-Hindawi, Bassam; Al-Sulaibi, Mazen A.M.; Meetani, Mohammad; Thiemann, Thies
Journal of Chemical Research, 2010 , # 6 p. 325 - 329
反应条件
sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid in dichloromethane
3 h; Ambient temperature;
参考文献
Blum. Jochanan; Ben-Shoshan, Shoshanna
Journal of Heterocyclic Chemistry, 1983 , vol. 20, p. 1461 - 1464
反应条件
1: 1.) hydrazine hydrate, 2.) KOH / 1.) triethylene glycol, 110 deg C, 60 min, 2.) 140 deg C, 2 h
2: 66 percent Chromat. / 2,3-dichloro-5,6-dicyano-1,4-benzoquinone (DDQ) / benzene / 5 h / Ambient temperature
View Scheme
参考文献
Oesch, Franz; Stillger, Gisela; Frank, Heinz; Platt, Karl L.
Journal of Organic Chemistry, 1982 , vol. 47, # 3 p. 568 - 571
反应条件
selenium
T=310 - 320°C;
参考文献
Fieser; Hershberg; Newman
Journal of the American Chemical Society, 1935 , vol. 57, p. 1509