反应条件
thionyl chloride; triethylamine 1.) dichloromethane, -60 - -50 deg C, 1 h, 2.) -50 - -40 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Sato, Kikumasa; Inoue, Seiichi; Ozawa, Kimio; Tazaki, Michiko
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , p. 2715 - 2719
