3-乙酰硫基-2-甲基丙酸合成路线 (共 5 条)
反应条件
in tetrahydrofuran Heating;
参考文献
Crich, David; Sana, Kasinath
Journal of Organic Chemistry, 2009 , vol. 74, # 9 p. 3389 - 3393
参考文献
Ghizzoni, Massimo; Haisma, Hidde J.; Dekker, Frank J.
European Journal of Medicinal Chemistry, 2009 , vol. 44, # 12 p. 4855 - 4861
反应条件
pyridine; thionyl chloride in toluene
1.5 h; Ambient temperature;
参考文献
Suh, John T.; Skiles, Jerry W.; Williams, Bruce E.; Youssefyeh, Raymond D.; Jones, Howard; et al.
Journal of Medicinal Chemistry, 1985 , vol. 28, # 1 p. 57 - 66
反应条件
chlorine in dichloromethane
T=-30°C;
参考文献
Vasil'eva, T. P.; Lin'kova, M. G.; Kil'disheva, O. V.; Knunyants, I. L.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1981 , vol. 30, # 1 p. 137 - 143
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1981 , # 1 p. 159 - 165
反应条件
cation-exchange resin PK-216 (H type)
T=65°C; 1 h;
参考文献
Sakimae, Akihiro; Ozaki, Eiji; Toyama, Hiroko; Ohsuga, Naoto; Numazawa, Ryozo; et al.
Bioscience, Biotechnology, and Biochemistry, 1993 , vol. 57, # 5 p. 782 - 786