苄基-(3-硝基-苯基)-胺合成路线 (共 24 条)
反应条件
sodium tris(acetoxy)borohydride in 1,2-dichloro-ethane T=20°C; pH=7; 24 h; Inert atmosphere;
参考文献
Kumar, Dinesh; Kommi, Damodara N.; Chebolu, Rajesh; Garg, Sanjeev K.; Kumar, Raj; Chakraborti, Asit K.
RSC Advances, 2013 , vol. 3, # 1 p. 91 - 98
反应条件
copper(l) iodide; TBAA; L-proline in N,N-dimethyl-formamide T=25°C; 24 h; Inert atmosphere;
参考文献
Yang, Chu-Ting; Fu, Yao; Huang, Yao-Bing; Yi, Jun; Guo, Qing-Xiang; Liu, Lei
Angewandte Chemie, International Edition, 2009 , vol. 48, # 40 p. 7398 - 7401
Angewandte Chemie, 2009 , vol. 121, # 40 p. 7534 - 7537
反应条件
potassium phosphate; copper monoiodide in ethylene glycol
参考文献
Buchwald, Stephen L.; Klapars, Artis; Antilla, Jon C.; Job, Gabriel E.; Wolter, Martina; Kwong, Fuk Y.; Nordmann, Gero; Hennessy, Edward J.
Patent: US2003/65187 A1, 2003 ;
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane 2 h; Reflux;
参考文献
King, Frank D.; Caddick, Stephen
Tetrahedron, 2013 , vol. 69, # 40 p. 8592 - 8601
反应条件
1H-imidazole; iodine; chloro-diphenylphosphine in dichloromethane 8 h; Reflux;
参考文献
Nowrouzi, Najmeh; Jonaghani, Mohammad Zareh
Canadian Journal of Chemistry, 2012 , vol. 90, # 6 p. 498 - 509
反应条件
nido-decaborane in methanol T=20°C; 2 h;
参考文献
Park, Eun Soo; Lee, Ji Hee; Kim, Soo Jung; Yoon, Cheol Min
Synthetic Communications, 2003 , vol. 33, # 19 p. 3387 - 3396
反应条件
triethylamine in dichloromethane 48 h; Heating;
参考文献
Pati, Hari; Weisbruch, Paul; Lemon, Adrienne; Lee, Moses
Synthetic Communications, 2004 , vol. 34, # 5 p. 933 - 940
反应条件
sulfuric acid; acetic acid; phenylacetylene 1) 1h, RT, 2) 2h, 70 deg C;
参考文献
Leardini, Rino; Nanni, Daniele; Tundo, Antonio; Zanardi, Giuseppe; Ruggieri, Fabrizio
Journal of Organic Chemistry, 1992 , vol. 57, # 6 p. 1842 - 1848
反应条件
T=-196°C; Irradiation;
参考文献
Leyva, Elisa; Munoz, Daniel; Platz, Matthew S.
Journal of Organic Chemistry, 1989 , vol. 54, # 25 p. 5938 - 5945
反应条件
sodium tetrahydroborate
参考文献
Mori,K. et al.
Chemical and Pharmaceutical Bulletin, 1971 , vol. 19, p. 1722 - 1727