1: With hydrogenchloride; sodium nitrite in water T=0°C; 0.166667 h; Inert atmosphere; 2: With sodium azide in water T=0 - 20°C; 2 h; Inert atmosphere;
参考文献
Van Kalkeren, Henri A.; Te Grotenhuis, Colet; Haasjes, Frank S.; Hommersom; Rutjes, Floris P. J. T.; Van Delft, Floris L.
European Journal of Organic Chemistry, 2013 , # 31 p. 7059 - 7066
1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 2 h / 0 °C / |Inert atmosphere
2: (Ph)2SiH2; P-(phenyl)dibenzophosphole / 1,4-dioxane / 44 h / 101 °C / |Inert atmosphere
View Scheme
参考文献
Van Kalkeren, Henri A.; Te Grotenhuis, Colet; Haasjes, Frank S.; Hommersom; Rutjes, Floris P. J. T.; Van Delft, Floris L.
European Journal of Organic Chemistry, 2013 , # 31 p. 7059 - 7066
