3,5-二氯-4-羟基苯甲酸合成路线 (共 36 条)
反应条件
hydrogenchloride; dihydrogen peroxide; acetic acid in water T=60°C; 4 h; Solvent;
参考文献
Mukhopadhyay; Chandalia
Organic Process Research and Development, 1999 , vol. 3, # 1 p. 10 - 16
反应条件
1: (2,6-dichlorophenoxy)triethylsilane With sec.-butyllithium in tetrahydrofuran; cyclohexane T=-75°C; 0.75 h; 2: carbon dioxide in tetrahydrofuran; cyclohexane
参考文献
Schlosser, Manfred; Heiss, Christophe; Marzi, Elena; Scopelliti, Rosario
European Journal of Organic Chemistry, 2006 , # 19 p. 4398 - 4404
参考文献
Gazzetta Chimica Italiana, , vol. 29 I, p. 387,388
参考文献
Journal of the American Chemical Society, , vol. 41, p. 2038
反应条件
hydrogen iodide T=130 - 140°C; im geschlossenen Rohr;
参考文献
Gazzetta Chimica Italiana, , vol. 29 II, p. 39
反应条件
1.1: 89 percent / triethylamine / tetrahydrofuran / 12 h / 50 °C 2.1: sec-butyllithium / cyclohexane; tetrahydrofuran / 0.75 h / -75 °C 2.2: cyclohexane; tetrahydrofuran View Scheme
参考文献
European Journal of Organic Chemistry, , # 19 p. 4398 - 4404
反应条件
sodium hydroxide; sodium hypochlorite T=20°C; 1 h; pH > 12; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), , # 6 p. 985 - 988
反应条件
1: lithium aluminum hydride 2: diazomethane View Scheme
参考文献
Chemosphere, , vol. 44, # 7 p. 1603 - 1616
反应条件
antimony(V) pentachloride
参考文献
Journal fuer Praktische Chemie (Leipzig), , vol. <2> 13, p. 427
参考文献
Gazzetta Chimica Italiana, , vol. 30 II, p. 491