(2-甲基磺酰基苯基)-甲醇合成路线 (共 16 条)
反应条件
dimethylsulfide; N-succinimide; triethylamine in toluene
参考文献
Journal of the American Chemical Society, , vol. 105, # 19 p. 6096 - 6103
反应条件
sodium methylselenolate in N,N,N',N',N'',N''-hexamethylphosphoric triamide 8 h; Heating;
参考文献
Evers, Michel; Christiaens, Leon
Tetrahedron Letters, 1983 , vol. 24, # 4 p. 377 - 380
反应条件
1: 61 percent 2: 1.67 h / 800 °C / 0 Torr View Scheme
参考文献
Cadogan, J. I. G.; Husband, James B.; McNab Hamish
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1983 , p. 697 - 702
反应条件
1: 83 percent / conc. hydrochloric acid / 1 h / Ambient temperature
2: 1.) triethyl phosphite, 2.) sodium methoxide / 1.) reflux, 20 min; 2.) DMF, 10 min
3: 76 percent / Raney nickel / ethanol / Heating
View Scheme
参考文献
Clark, Peter David; Ewing, David F.; Kerrigan, Frank; Scrowston, Richard M.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1982 , p. 615 - 622
反应条件
perchloric acid; dihydrogen peroxide in ethanol; water
T=25°C; Rate constant;
参考文献
Luedersdorf,R.; Praefcke,K.
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1976 , vol. <b> 31, p. 1658 - 1661
反应条件
in ethanol
T=20°C; Rate constant;
参考文献
Ruff, Ferenc; Kucsman, Arpad
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1988 , p. 1123 - 1128