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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
33397-21-6
合成路线
（共 146 条）
33397-21-6
+
4635-59-0
4-氯丁酰氯
→
反应条件
40877-19-8
Γ-氯-4-甲氧基苯丁酮
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
141-30-0
3,6-二氯哒嗪
+
33397-21-6
→
反应条件
2132-80-1
4,4-二甲氧基联苯
+
58059-31-7
3-氯-6-(4-甲氧苯基)哒嗪
反应条件
palladium diacetate; triphenylphosphine; cesium fluoride in N,N-dimethyl-formamide T=90°C; Inert atmosphere; chemoselective reaction;
参考文献
European Journal of Organic Chemistry, , # 1 p. 117 - 124
141-30-0
3,6-二氯哒嗪
+
33397-21-6
→
反应条件
58059-31-7
3-氯-6-(4-甲氧苯基)哒嗪
反应条件
palladium diacetate; triphenylphosphine; cesium fluoride in N,N-dimethyl-formamide T=90°C; Inert atmosphere; Reagent/catalyst; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
33397-21-6
+
135034-10-5
3-氯-6-碘哒嗪
→
反应条件
58059-31-7
3-氯-6-(4-甲氧苯基)哒嗪
反应条件
palladium diacetate; triphenylphosphine in N,N-dimethyl-formamide T=90°C; 4 h; Inert atmosphere; Catalytic behavior; Reagent/catalyst; chemoselective reaction;
参考文献
Urgin, Karene; Aube, Christophe; Pipelier, Muriel; Blot, Virginie; Thobie-Gautier, Christine; Sengmany, Stephane; Lebreton, Jacques; Leonel, Eric; Dubreuil, Didier; Condon, Sylvie
European Journal of Organic Chemistry, 2013 , # 1 p. 117 - 124
33397-21-6
+
1711-06-4
间甲基苯甲酰氯
→
反应条件
53039-63-7
(4-甲氧基苯基)(3-甲基苯基)甲酮
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
5271-67-0
2-噻吩甲酰氯
+
33397-21-6
→
反应条件
4160-63-8
2-(4-甲氧基苄氧基)噻吩
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
33397-21-6
+
141-75-3
丁酰氯
→
反应条件
4160-51-4
4'-甲氧基苯丁酮
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
33397-21-6
+
138313-22-1
→
反应条件
2132-80-1
4,4-二甲氧基联苯
+
182169-63-7
1-(4-甲氧基[1,1-联苯]-3-基)乙酮
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
577-19-5
1-溴-2-硝基苯
+
33397-21-6
→
反应条件
20013-55-2
4'-甲氧基-2-硝基联苯
+
2132-80-1
4,4-二甲氧基联苯
反应条件
caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 2 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
33397-21-6
+
98-88-4
苯甲酰氯
→
反应条件
611-94-9
4-甲氧基二苯甲酮
反应条件
triethylamine; tetrakis(triphenylphosphine) palladium(0) in 1,4-dioxane T=80°C; 3 h;
参考文献
Rao, Maddali L.N.; Venkatesh, Varadhachari; Banerjee, Debasis
Tetrahedron, 2007 , vol. 63, # 52 p. 12917 - 12926
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