(S)-(-)-3-羟基-3-苯基丙酸乙酯合成路线 (共 48 条)
反应条件
hydrogen; Ru(R-Xyl-P-Phos)(C6H6)Cl2 in ethanol; dichloromethane T=90°C; P=15514.4 Torr; 2 h;
参考文献
Wu, Jing; Chen, Hua; Kwok, Wai Him; Lam, Kim Hung; Zhou, Zhong Yuan; Yeung, Chi Hung; Chan, Albert S.C
Tetrahedron Letters, 2002 , vol. 43, # 8 p. 1539 - 1543
反应条件
NaBO3 in tetrahydrofuran; water T=20°C;
参考文献
Lee, Ji-Eon; Yun, Jaesook
Angewandte Chemie - International Edition, 2008 , vol. 47, # 1 p. 145 - 147
反应条件
hydrogen; C50H44Cl2N2O8P4Ru(4-)*Zr(4+) in methanol T=20°C; P=72402.6 Torr; 20 h; Product distribution / selectivity;
参考文献
Lin, Wenbin; Hu, Aiguo; Ngo, Helen L.
Patent: US2004/192543 A1, 2004 ;
Location in patent: Page/Page column 9 ;
反应条件
Candida rugose type VII lipase in octane T=25°C; Molecular sieveEnzymatic reaction; optical yield given as percent eeenantioselective reaction;
参考文献
Tetrahedron Asymmetry, , vol. 22, # 16-17 p. 1672 - 1679
反应条件
indium; CD 1.) THF, a) 0 deg C, 30 min, b) 18 deg C, 20 min, 2.) pentane, -75 to 18 deg C, 15 h; Yield given. Multistep reaction. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), , # 6 p. 711 - 714
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethanol P=760 Torr; 1.5 h;
参考文献
Cabon; Buisson; Larcheveque; Azerad
Tetrahedron Asymmetry, 1995 , vol. 6, # 9 p. 2199 - 2210
反应条件
hydrogen; triethylamine; palladium on activated charcoal in ethanol P=760 Torr; 1.5 h;
参考文献
Cabon; Buisson; Larcheveque; Azerad
Tetrahedron Asymmetry, 1995 , vol. 6, # 9 p. 2199 - 2210
反应条件
immobilized Candida parapsilosis ATCC 7330 in ethanol; water T=25°C; 6 h;
参考文献
Padhi, Santosh Kumar; Titu; Pandian, N. Ganesh; Chadha, Anju
Tetrahedron, 2006 , vol. 62, # 21 p. 5133 - 5140
反应条件
potassium hydrogencarbonate in acetone 36 h; Heating;
参考文献
Boaz, Neil W.
Journal of Organic Chemistry, 1992 , vol. 57, # 15 p. 4289 - 4292
反应条件
hydrogen; boric acid; nickel in methanol; water 4 h;
参考文献
Bernardi, Anna; Colombo, Lino; Gennari, Cesare; Prati, Laura
Tetrahedron, 1984 , vol. 40, # 19 p. 3769 - 3776