2-(四氢呋喃-2-基)乙腈合成路线 (共 10 条)
反应条件
in dimethyl sulfoxide T=80°C; 3.5 h;
参考文献
Erickson, Shawn David; Baldwin, John J.; Dolle III, Roland Ellwood; Inglese, James; Ohlmeyer, Michael H.J.; Ho, Koc-Kan; Bohnstedt, Adolph C.; Kultgen, Steven G.; Conti, Paolo Giovanni Martino; Leysen, Dirk; van der Louw, Jaap
Patent: US2004/87601 A1, 2004 ;
Location in patent: Page 27 ;
US 20040087601 A1
反应条件
in ethanol 10 h; Heating;
参考文献
Laxmi, Y. R. Santosh; Iyengar, D. S.
Synthesis, 1996 , # 5 p. 594 - 596
反应条件
1: 93 percent / KOH 2: 93 percent / ethanol / 10 h / Heating View Scheme
参考文献
Synthesis, , # 5 p. 594 - 596
参考文献
Journal of the American Chemical Society, , vol. 68, p. 2743
参考文献
Journal of the Chemical Society, , p. 718,720
反应条件
sodium hydride 1.) dioxane, 5 deg C, 2.) dioxane, 25 deg C, 2 h; Yield given. Multistep reaction;
参考文献
Bollettino Chimico Farmaceutico, , vol. 132, # 5 p. 150 - 152
参考文献
Journal of Organic Chemistry, , vol. 69, # 4 p. 1331 - 1336
反应条件
1: 97 percent / KOH 2: 91 percent / H2SO4 / 5 h / Heating View Scheme
参考文献
Laxmi, Y. R. Santosh; Iyengar, D. S.
Synthesis, 1996 , # 5 p. 594 - 596
参考文献
Synthesis, , # 5 p. 594 - 596
反应条件
borane-THF in tetrahydrofuran
T=20°C; 2 h;
参考文献
Erickson, Shawn David; Baldwin, John J.; Dolle III, Roland Ellwood; Inglese, James; Ohlmeyer, Michael H.J.; Ho, Koc-Kan; Bohnstedt, Adolph C.; Kultgen, Steven G.; Conti, Paolo Giovanni Martino; Leysen, Dirk; van der Louw, Jaap
Patent: US2004/87601 A1, 2004 ;
Location in patent: Page 27 ;
US 20040087601 A1