2,2′-二吡啶基 N-氧化物合成路线 （共 35 条）
参考文献
Chen, Zhuqi; Ding, Fei; Hao, Feng; Guan, Ming; Bian, Zuqiang; Ding, Bei; Huang, Chunhui
New Journal of Chemistry, 2010 , vol. 34, # 3 p. 487 - 494
反应条件
trichlorophosphate 12 h; Heating;
参考文献
Araki, Koji; Mutai, Toshiki; Shigemitsu, Yasuhiro; Yamada, Masaki; Nakajima, Takayoshi; et al.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1996 , # 4 p. 613 - 618
反应条件
sulfuric acid; potassium nitrate T=80°C; 30 h;
参考文献
Zalas; Gierczyk; Klein; Siuzdak; Pedzinski; Luczak
Polyhedron, 2014 , vol. 67, p. 381 - 387
参考文献
FMC Corporation
Patent: US4808722 A1, 1989 ;
反应条件
1: 49 percent / HNO3; H2SO4 / 31 h / 100 °C 2: acetyl bromide View Scheme
参考文献
Zalas, Maciej; Gierczyk, Blazej; Ceglowski, Michal; Schroeder, Grzegorz
Chemical Papers, 2012 , vol. 66, # 8 p. 733 - 740
反应条件
1: HNO3; H2SO4 2: 95 percent / NaBH4 / Pd/C / methanol / cooling View Scheme
参考文献
Nguyen, Tuan Q.; Qu, Fanqi; Huang, Xiaoling; Janzen, Alexander F.
Canadian Journal of Chemistry, 1992 , vol. 70, # 7 p. 2089 - 2093
反应条件
1.1: 65 percent / KNO3; H2SO4 / 2.5 h / 110 °C 2.1: 88 percent / methanol / 0.5 h / 40 °C 3.1: LTMP / tetrahydrofuran / 1.5 h / -70 °C 3.2: 94 percent / I2 / tetrahydrofuran / 1 h / -70 °C 4.1: 64 percent / PBr3 / CHCl3 / 0.75 h / Heating View Scheme
参考文献
Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Gal, Catherine Le; Mongin, Florence; Queguiner, Guy
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2892 - 2897
反应条件
1.1: LDA / hexane; tetrahydrofuran / 0.5 h / -70 °C 1.2: 70 percent / BrCN / hexane; tetrahydrofuran / 0.25 h / -70 °C 2.1: 66 percent / KNO3; conc. H2SO4 / 20 h / 80 °C View Scheme
参考文献
Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Gal, Catherine Le; Mongin, Florence; Queguiner, Guy
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2892 - 2897
反应条件
1.1: 65 percent / KNO3; H2SO4 / 2.5 h / 110 °C 2.1: 88 percent / methanol / 0.5 h / 40 °C 3.1: LDA / hexane; tetrahydrofuran / 1 h / -70 °C 3.2: 15 percent / BrCN / hexane; tetrahydrofuran / 0.25 h / -70 °C 4.1: 90 percent / PBr3 / CHCl3 / 0.75 h / Heating View Scheme
参考文献
Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Gal, Catherine Le; Mongin, Florence; Queguiner, Guy
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2892 - 2897
反应条件
1: With lithium diisopropyl amide in tetrahydrofuran; hexane T=-70°C; Metallation; 0.5 h; 2: With bromocyane in tetrahydrofuran; hexane T=-70°C; Bromination; 0.25 h;
参考文献
Trecourt, Francois; Gervais, Bruno; Mongin, Olivier; Gal, Catherine Le; Mongin, Florence; Queguiner, Guy
Journal of Organic Chemistry, 1998 , vol. 63, # 9 p. 2892 - 2897
