1,1,2,2,9,9,10,10-八氟[2.2]二聚对二甲苯合成路线 （共 23 条）
反应条件
1.1: 82 percent / iron; hydrochloric acid / ethanol; H2O / 4 h / Heating 2.1: H2SO4; NaNO2 / acetic acid; H2O / 2 h / 0 °C 2.2: 6 percent / copper(I) bromide; hydrobromic acid / H2O; acetic acid / 1 h / 70 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 25 p. 9137 - 9143
反应条件
1.1: 77 percent / iron; hydrochloric acid / ethanol; H2O / 4 h / Heating 2.1: H2SO4; NaNO2 / acetic acid; H2O / 2 h / 0 °C 2.2: 6 percent / copper(I) bromide; hydrobromic acid / H2O; acetic acid / 1 h / 70 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 25 p. 9137 - 9143
反应条件
palladium dichloride in tetrahydrofuran Phenylation; reduction; 16 h; Heating;
参考文献
Journal of Organic Chemistry, , vol. 64, # 25 p. 9137 - 9143
反应条件
1.1: H2SO4; NaNO2 / acetic acid; H2O / 2 h / 0 °C 1.2: 78 percent / potassium iodide / H2O; acetic acid / 1 h / 70 °C 2.1: 9 percent / palladium dichloride / tetrahydrofuran / 16 h / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 64, # 25 p. 9137 - 9143
反应条件
1: 55 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation 2: Cu / 640 °C 3: toluene / 110 °C View Scheme
参考文献
Russian Journal of Organic Chemistry, , vol. 29, # 10 p. 1663 - 1665
Zhurnal Organicheskoi Khimii, , vol. 29, # 10 p. 1999 - 2001
反应条件
calcium chloride; zinc in N,N-dimethyl acetamide T=120 - 140°C; 4 h; Catalytic behavior; Reagent/catalyst;
参考文献
LIN, Chun-Hsu; SUN, Chien-Yi; YIN, Yung-Yu; LI, Chun-Shih; CHOU, Yo-Chun
Patent: US2014/11986 A1, 2014 ;
Location in patent: Paragraph 0048 ;
反应条件
in anhydrous butyl ether T=110°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 72, # 2 p. 550 - 558
反应条件
1: 48 percent / Mg / dimethylformamide / 0.5 h / 20 °C 2: 53 percent / CsF; Pd2(dba)3*CHCl3; 4-tert-butylcatechol / methoxybenzene / 24 h / 160 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 66, # 21 p. 7216 - 7218
反应条件
1: 88 percent / SF4 / 150 °C 2: 78 percent / N-bromosuccinimide / CCl4 / Heating; Irradiation 3: 31.8 percent / TiCl4, LiAlH4 / tetrahydrofuran / Heating View Scheme
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1827 - 1830
反应条件
lithium aluminium tetrahydride; titanium tetrachloride in tetrahydrofuran Heating;
参考文献
Journal of Organic Chemistry, , vol. 58, # 7 p. 1827 - 1830
