环丙基二苯基锍四氟硼酸盐合成路线 （共 14 条）
反应条件
potassium tert-butylate in tetrahydrofuran; dimethyl sulfoxide T=20°C; 0.833333 h;
参考文献
Jenkins, Ian D.; Lacrampe, Fabienne; Ripper, Justin; Alcaraz, Lilian; Van Le, Phuc; Nikolakopoulos, George; De Leone, Priscila Almeida; White, Rodney H.; Quinn, Ronald J.
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1304 - 1313
反应条件
tetrafluoroboric acid; sodium in tetrahydrofuran; dichloromethane; water
反应条件
potassium hydroxide in dimethyl sulfoxide 24 h; Ambient temperature;
参考文献
Lightner,D.A.; Chang,T.C.; Hefelfinger,D.
Journal of the American Chemical Society, 1985 , vol. 107, p. 7499
反应条件
KO-t-Bu in tetrahydrofuran addn. of KO-t-Bu to the Fe compd. and S compd. in THF (inert atmosphere) and stirring for 18 h at 20°C; filtn., evapn. (vacuum), dissolving in petroleum ether, concg. and crystn. at -28°C; elem. anal.;
参考文献
Weber, Lothar; Luecke, Ewald; Boese, Roland
Organometallics, 1988 , vol. 7, p. 978 - 983
反应条件
KO-t-Bu in tetrahydrofuran addn. of KO-t-Bu in THF to the Fe compd. and P compd. in THF (inert atmosphere); filtn., evapn. (vacuum), soln. in petroleum ether, concn. and standing at -28°C; elem. anal.;
参考文献
Weber, Lothar; Luecke, Ewald; Boese, Roland
Organometallics, 1988 , vol. 7, p. 978 - 983
反应条件
potassium hydroxide in dimethyl sulfoxide
参考文献
Trost,B.M.; Bogdanowicz,M.J.
Journal of the American Chemical Society, 1973 , vol. 95, p. 5321 - 5334
反应条件
sodium hydride in ethylene glycol dimethyl ether; dimethyl sulfoxide
参考文献
Trost,B.M.; Bogdanowicz,M.J.
Journal of the American Chemical Society, 1973 , vol. 95, p. 5298 - 5307
反应条件
(i) KOH, DMSO, (ii) aq. HBF4; Multistep reaction;
参考文献
Trost,B.M.; Bogdanowicz,M.J.
Journal of the American Chemical Society, 1973 , vol. 95, p. 5321 - 5334
反应条件
Yield given. Multistep reaction;
参考文献
Paquette,L.A.; Weber,J.C.; Kobayashi,T.
Journal of the American Chemical Society, 1988 , vol. 110, p. 8591
参考文献
Hanack,M. et al.
Journal of the American Chemical Society, 1979 , vol. 101, p. 100 - 108
