2,(4-甲酰-3-甲基噻吩-2-基)乙基醋酸盐合成路线 （共 11 条）
反应条件
1: 43 percent / AcOH; AcONH4; 3 Angstroem molecular sieves / toluene / 6 h / Heating 2: 82 percent / Na2S; AcOH / ethanol / 2 h / -40 - -10 °C 3: 93 percent / CuBr2; t-BuONO / acetonitrile / 0.5 h / 0 °C 4: 94 percent / Zn; AcOH / 16 h / Heating 5: 81 percent / LiAlH4 / diethyl ether / 3 h / Heating 6: 74 percent / MnO2 / CHCl3 / 5 h / 20 °C View Scheme
参考文献
Hawksley, Daniel; Griffin, David A.; Leeper, Finian J.
Journal of the Chemical Society. Perkin Transactions 1, 2001 , # 2 p. 144 - 148
