1-(2-萘基)-1-戊酮合成路线 (共 17 条)
反应条件
1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; triethylamine / 20 h / 50 °C / |Inert atmosphere 2: tetrahydrofuran / 16 h / 20 °C 3: AgNTf2; {1,3-bis[2,6-di(propan-2-yl)phenyl]-1,3-dihydro-2H-imidazol-2-ylidene}AuCl / dichloromethane / 2 h / 20 °C / |Inert atmosphere View Scheme
参考文献
Lauterbach, Tobias; Arndt, Sebastian; Rudolph, Matthias; Rominger, Frank; Hashmi, A. Stephen K.
Advanced Synthesis and Catalysis, 2013 , vol. 355, # 9 p. 1755 - 1761
反应条件
water; methyl iodide 1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, room temperature; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mortier, Jacques; Vaultier, Michel; Plunian, Barbara; Sinbandhit, Sourisak
Canadian Journal of Chemistry, 1999 , vol. 77, # 1 p. 98 - 112
反应条件
1: AlCl3 2: sulfur / 220 °C View Scheme
参考文献
Koelbel
Brennstoff-Chemie, 1949 , vol. 30, p. 73,75
反应条件
1: AlCl3 2: sulfur / 220 °C View Scheme
参考文献
Koelbel
Brennstoff-Chemie, 1949 , vol. 30, p. 73,75
反应条件
1.) THF, hexane, -78 deg C, 1 h, 2.) THF, hexane, -78 deg C; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Mortier, Jacques; Vaultier, Michel; Plunian, Barbara; Sinbandhit, Sourisak
Canadian Journal of Chemistry, 1999 , vol. 77, # 1 p. 98 - 112
反应条件
1,3-dithiane polymer supported synthesis; Yield givenMultistep reaction. Yields of byproduct given;
参考文献
Bertini, Vincenzo; Lucchesini, Francesco; Pocci, Marco; De Munno, Angela
Tetrahedron Letters, 1998 , vol. 39, # 50 p. 9263 - 9266
参考文献
Arrowsmith,G.B. et al.
Journal of the Chemical Society, 1965 , p. 2072 - 2078