5-羟基甲基-N,N-二甲基色胺合成路线 （共 5 条）
反应条件
hydrogen; [Rh DiPFc (COD) ] BF4 in methanol T=20°C; P=10343.2 Torr; 18 h;
参考文献
CIBA SPECIALTY CHEMICALS HOLDING INC.
Patent: WO2004/56769 A2, 2004 ;
Location in patent: Page 54 ;
反应条件
lithium aluminium tetrahydride in tetrahydrofuran 2 h; Heating;
参考文献
Skwierawska; Paluszkiewicz
Polish Journal of Chemistry, 2003 , vol. 77, # 3 p. 329 - 332
反应条件
1.1: NaNO2*H2O; aq. HCl / -10 °C 1.2: SnCl2*2H2O; aq. HCl 2.1: 34 percent / H2SO4 conc. / toluene / 6 h / Heating 3.1: 77 percent / ethanol; H2O / 6 h / 50 °C 4.1: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Skwierawska; Paluszkiewicz
Polish Journal of Chemistry, 2003 , vol. 77, # 3 p. 329 - 332
反应条件
1: 34 percent / H2SO4 conc. / toluene / 6 h / Heating 2: 77 percent / ethanol; H2O / 6 h / 50 °C 3: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Skwierawska; Paluszkiewicz
Polish Journal of Chemistry, 2003 , vol. 77, # 3 p. 329 - 332
反应条件
1: 77 percent / ethanol; H2O / 6 h / 50 °C 2: 95 percent / LiAlH4 / tetrahydrofuran / 2 h / Heating View Scheme
参考文献
Skwierawska; Paluszkiewicz
Polish Journal of Chemistry, 2003 , vol. 77, # 3 p. 329 - 332
