N-甲氧基-1-(4-硝基苯基)甲亚胺合成路线 （共 6 条）
反应条件
manganese(IV) oxide; 4 A molecular sieve in dichloromethane 22 h; Heating;
参考文献
Kanno, Hisashi; Taylor, Richard J. K.
Synlett, 2002 , # 8 p. 1287 - 1290
参考文献
Shirokane, Kenji; Wada, Takamasa; Yoritate, Makoto; Minamikawa, Ryo; Takayama, Nobuaki; Sato, Takaaki; Chida, Noritaka
Angewandte Chemie - International Edition, 2014 , vol. 53, # 2 p. 512 - 516
Angew. Chem., 2014 , vol. 126, # 2 p. 522 - 526,5
反应条件
sodium hydride 1.) DMF, room temp., 10 min, 2.) DMF, 30 min; Yield given. Multistep reaction;
参考文献
Mauleon, David; Granados, Ricardo; Minguillon, Cristina
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3105 - 3106
反应条件
sodium hydride in N,N-dimethyl-formamide 1 h; Ambient temperature;
参考文献
Mauleon, David; Granados, Ricardo; Minguillon, Cristina
Journal of Organic Chemistry, 1983 , vol. 48, # 18 p. 3105 - 3106
反应条件
(i) B2H6, THF, (ii) aq. KOH; Multistep reaction;
参考文献
Feuer,H.; Braunstein,D.M.
Journal of Organic Chemistry, 1969 , vol. 34, # 6 p. 1817 - 1821
反应条件
1: dipotassium peroxodisulfate; palladium diacetate; trifluoroacetic acid / 15 h / 120 °C / Inert atmosphere
2: hydrogenchloride; water / 100 °C / Inert atmosphere
View Scheme
参考文献
Thirunavukkarasu, Vedhagiri S.; Cheng, Chien-Hong
Chemistry - A European Journal, 2011 , vol. 17, # 52 p. 14723 - 14726
