2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 合成路线 （共 6 条）
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反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃
反应条件
fluorspar; cobalt(III) fluoride T=440°C; in nickel tube;
参考文献
Chambers, Richard D.; Grievson, Brian; Drakesmith, Frederick G.; Powell, Richard L.
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反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 + 308-48-5 1,1,1,2,2,3,3,4,4-九氟-4-(1,1,2,2,3,3,4,4,4-九氟丁氧基)丁烷 +
反应条件
hydrogen fluoride T=5 - 6°C; 7.2 h; electrochemical cell; Yield given. Further byproducts given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
→
反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 +
反应条件
hydrogen fluoride T=5 - 6°C; 6.7 h; electrochemical cell; Title compound not separated from byproducts;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
→
反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 +
反应条件
hydrogen fluoride T=5 - 6°C; 7.2 h; electrochemical cell; Yield given. Further byproducts given. Yields of byproduct given;
参考文献
Abe, Takashi; Hayashi, Eiji; Baba, Hajime; Kodaira, Kazuo; Nagase, Shunji
→
反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 +
反应条件
in hydrogen fluoride T=5°C; 77 h; electrochemical fluorination;
参考文献
Napoli, M.; Conte, L.; Gambaretto, G. P.; Carlini, F. M.
→
反应条件
335-35-3 2,2,3,3,4,4,5,5,6-九氟-6-(1,1,2,2,3,3,3-七氟丙基)四氢吡喃 +
反应条件
hydrogen fluoride T=5°C; 192 h; elecrochemical fluorination; anode and cathode: nickel foam; anode pot. versus reference electrode 4.30 V; Yield given. Yields of byproduct given;
参考文献
Drakesmith, F. G.; Hughes, D. A.
