邻苯二亚胺甲基磷酸二乙酯合成路线 （共 14 条）
反应条件
hydrogenchloride; hydrazine hydrate 1.) MeOH, overnight, room temp.; 2 h, reflux, 2.) 6 h, reflux; Multistep reaction;
参考文献
Cameron, David G.; Hudson, Harry R.; Pianka, Max
Phosphorus, Sulfur and Silicon and the Related Elements, 1993 , vol. 83, # 1-4 p. 21 - 38
反应条件
1: N2H4*H2O / ethanol / 84 h / Ambient temperature
2: Et3N / CHCl3 / 15 h / Ambient temperature
View Scheme
参考文献
Hirschmann, Ralph; Yager, Kraig M.; Taylor, Carol M.; Witherington, Jason; Sprengeler, Paul A.; Phillips, Barton W.; Moore, William; Smith III, Amos B.
Journal of the American Chemical Society, 1997 , vol. 119, # 35 p. 8177 - 8190
参考文献
Slater, Martin J.; Laws, Andrew P.; Page, Michael I.
Bioorganic Chemistry, 2001 , vol. 29, # 2 p. 77 - 95
反应条件
hydrazine in ethanol
T=20°C; Heating / reflux;
参考文献
Board of Regents the University of Texas System
Patent: US6746662 B1, 2004 ;
Location in patent: Page column 7; 8 ;
