2-(2'-甲酰基-4'-硝基苯氧基)己酸甲酯合成路线 (共 6 条)
反应条件
1: With sulfuric acid T=5°C; 0.25 h; 2: T=5°C; 2 h;
参考文献
Rhodia Chimie
Patent: US6855842 B1, 2005 ;
Location in patent: Page/Page column 16 ;
反应条件
potassium carbonate in N,N-dimethyl-formamide T=92 - 94°C; 3.5 h;
参考文献
Kwiecien
Polish Journal of Chemistry, 2004 , vol. 78, # 10 p. 1865 - 1869
反应条件
1: NaOH / 0.5 h / 90 °C 2: 87 percent / K2CO3 / dimethylformamide / 3.5 h / 92 - 94 °C View Scheme
参考文献
Kwiecien
Polish Journal of Chemistry, 2004 , vol. 78, # 10 p. 1865 - 1869
反应条件
1: NaOH / 2 h / 50 °C 2: 87 percent / K2CO3 / dimethylformamide / 3.5 h / 92 - 94 °C View Scheme
参考文献
Kwiecien
Polish Journal of Chemistry, 2004 , vol. 78, # 10 p. 1865 - 1869
反应条件
1: 80 percent / NaOH / Heating 2: acetic anhydride; sodium acetate; acetic acid / 3 h / Heating View Scheme
参考文献
Kwiecien
Polish Journal of Chemistry, 2004 , vol. 78, # 10 p. 1865 - 1869
反应条件
sodium hydroxide Heating;
参考文献
Kwiecien
Polish Journal of Chemistry, 2004 , vol. 78, # 10 p. 1865 - 1869