2-环己烯-1-基苯甲酸酯合成路线 （共 25 条）
反应条件
1: 99 percent / CeCl3*H2O, NaBH4 / methanol / 0.17 h 2: 93 percent / DMAP / CH2Cl2 / 24 h / Heating 3: tributyltin hydride, AIBN / benzene / 8 h / Heating View Scheme
参考文献
Crich, David; Yao, Qingwei; Filzen, G. Fredrick
Journal of the American Chemical Society, 1995 , vol. 117, # 46 p. 11455 - 11470
反应条件
1: N-chloro-succinimide; tin(IV) chloride; water / acetonitrile / 18 h / 25 °C 2: triethylamine / dichloromethane View Scheme
参考文献
Tay, Daniel Weiliang; Tsoi, Ivan Tan; Er, Jun Cheng; Leung, Gulice Yiu Chung; Yeung, Ying-Yeung
Organic Letters, 2013 , vol. 15, # 6 p. 1310 - 1313
参考文献
Shi, Erbo; Shao, Ying; Chen, Shulin; Hu, Huayou; Liu, Zhaojun; Zhang, Jie; Wan, Xiaobing
Organic Letters, 2012 , vol. 14, # 13 p. 3384 - 3387
反应条件
1: 78 percent / NBS, water / tetrahydrofuran 2: 95 percent / pyridine / 24 h / Ambient temperature 3: 84 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 3 h / 120 °C View Scheme
参考文献
Gupta, Ajay K.; Kazlauskas, Romas J.
Tetrahedron: Asymmetry, 1993 , vol. 4, # 5 p. 879 - 888
反应条件
1: Ti(OPr-i)4 / CH2Cl2; 2,2,4-trimethyl-pentane / 0 °C 2: pyridine / CH2Cl2 / -30 °C 3: NaI / CH2Cl2; dimethylformamide / 0.33 h View Scheme
参考文献
Martin, Victor S.; Ode, Jesus M.; Palazon, Jose M.; Soler, Marcos A.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 4 p. 573 - 580
反应条件
1: pyridine / CH2Cl2 / -30 °C 2: NaI / CH2Cl2; dimethylformamide / 0.33 h View Scheme
参考文献
Martin, Victor S.; Ode, Jesus M.; Palazon, Jose M.; Soler, Marcos A.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 4 p. 573 - 580
反应条件
1: Ti(OPr-i)4 / CH2Cl2; 2,2,4-trimethyl-pentane / 0 °C 2: pyridine / CH2Cl2 / -30 °C 3: NaI / CH2Cl2; dimethylformamide / 0.33 h View Scheme
参考文献
Martin, Victor S.; Ode, Jesus M.; Palazon, Jose M.; Soler, Marcos A.
Tetrahedron: Asymmetry, 1992 , vol. 3, # 4 p. 573 - 580
反应条件
1: tetra-(n-butyl)ammonium iodide / water / 24 h / 40 °C 2: copper(I) bromide / dichloromethane; water / 36 h / 40 °C View Scheme
参考文献
Wei, Wei; Zhang, Chao; Xu, Yuan; Wan, Xiaobing
Chemical Communications, 2011 , vol. 47, # 38 p. 10827 - 10829
反应条件
1.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 °C / |Inert atmosphere 1.2: -45 °C / |Inert atmosphere 2.1: tetrahydrofuran; toluene / -45 °C / |Inert atmosphere View Scheme
参考文献
Wommack, Andrew J.; Kingsbury, Jason S.
Journal of Organic Chemistry, 2013 , vol. 78, # 21 p. 10573 - 10587
反应条件
1: 95 percent / pyridine / 24 h / Ambient temperature 2: 84 percent / 1,8-diazabicyclo<5.4.0>undec-7-ene (DBU) / 3 h / 120 °C View Scheme
参考文献
Gupta, Ajay K.; Kazlauskas, Romas J.
Tetrahedron: Asymmetry, 1993 , vol. 4, # 5 p. 879 - 888
