1-吡咯烷-1-基丁烷-1-酮合成路线 (共 7 条)
反应条件
NiII chloride hexahydrate in para-xylene T=155°C; 18 h; Inert atmosphere;
参考文献
Allen, C. Liana; Davulcu, Simge; Williams, Jonathan M. J.
Organic Letters, 2010 , vol. 12, # 22 p. 5096 - 5099
反应条件
in dichloromethane T=21°C; 16 h;
参考文献
Chudasama, Vijay; Akhbar, Ahmed R.; Bahou, Karim A.; Fitzmaurice, Richard J.; Caddick, Stephen
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7301 - 7317
反应条件
hydrogen in ethylene glycol dimethyl ether T=160°C; P=22502.3 Torr; 20 h; Inert atmosphereAutoclaveMolecular sieve;
参考文献
Stein, Mario; Breit, Bernhard
Angewandte Chemie - International Edition, 2013 , vol. 52, # 8 p. 2231 - 2234
反应条件
in dichloromethane T=21°C; 16 h;
参考文献
Chudasama, Vijay; Akhbar, Ahmed R.; Bahou, Karim A.; Fitzmaurice, Richard J.; Caddick, Stephen
Organic and Biomolecular Chemistry, 2013 , vol. 11, # 42 p. 7301 - 7317
反应条件
lipase of Horse Liver Acetonic Powder T=40°C; 24 h; enzymatic acylation of secondary cyclic amines with various lipases; Product distribution;
参考文献
Djeghaba, Zeineddine; Deleuze, Herve; Maillard, Bernard; Jeso, Bernard De
Bulletin des Societes Chimiques Belges, 1995 , vol. 104, # 3 p. 161 - 164
反应条件
in various solvent(s) T=40°C; lipase of Horse Liver Acetonic Powder;
参考文献
Djeghaba, Zeineddine; Deleuze, Herve; Maillard, Bernard; Jeso, Bernard De
Bulletin des Societes Chimiques Belges, 1995 , vol. 104, # 3 p. 161 - 164
反应条件
pyridine 0.5 h; Heating;
参考文献
Bellec, Christian; Gaurat, Olivier
Canadian Journal of Chemistry, 2004 , vol. 82, # 8 p. 1289 - 1293