(2Z,4E,6Z,8E)-3,7-二甲基-9-(2,6,6-三甲基-3-氧代-1-环己烯基)壬-2,4,6,8-四烯醛合成路线 (共 28 条)
反应条件
1: 17 percent / pyridinium dichromate, pyridinium trifluoroacetate / CH2Cl2 / 2 h / Ambient temperature 2: 50 percent / 40percent methylamine / benzene; H2O / 0.08 h / Ambient temperature View Scheme
参考文献
Helvetica Chimica Acta, , vol. 63, # 6 p. 1391 - 1395
反应条件
phosphoric acid; lead dioxide in tetrahydrofuran; water 0.5 h; Ambient temperature;
参考文献
Gieren, Alfred; Lamm, Viktor; Oesterhelt, Dieter; Schlude, Hans-Joerg
Zeitschrift fuer Naturforschung, Teil B: Anorganische Chemie, Organische Chemie, 1982 , vol. 37, # 12 p. 1612 - 1622
反应条件
manganese(IV) oxide; pentane
参考文献
Journal of the Chemical Society, , p. 4909
反应条件
1: 70 percent / manganese dioxide; acetic acid; sodium cyanide / 4 - 20 °C 2: 87 percent / potassium hydroxide / methanol; H2O / 14 h / Heating View Scheme
参考文献
Mironova; Leont'eva; Shevyakov; Alexeeva; Shvets; Demina; Krasnokutskaya; Finkel'shtein; Khodonov
Russian Journal of Bioorganic Chemistry, 2002 , vol. 28, # 6 p. 487 - 493
反应条件
1: 70 percent / manganese dioxide; acetic acid; sodium cyanide / 4 - 20 °C 2: 87 percent / potassium hydroxide / methanol; H2O / 14 h / Heating View Scheme
参考文献
Mironova; Leont'eva; Shevyakov; Alexeeva; Shvets; Demina; Krasnokutskaya; Finkel'shtein; Khodonov
Russian Journal of Bioorganic Chemistry, 2002 , vol. 28, # 6 p. 487 - 493
参考文献
Waldmann, Doris; Koenig, Thorsten; Schreier, Peter
Zeitschrift fuer Naturforschung, B: Chemical Sciences, 1995 , vol. 50, # 4 p. 589 - 594
反应条件
1: 70 percent / manganese dioxide; acetic acid; sodium cyanide / 4 - 20 °C 2: 87 percent / potassium hydroxide / methanol; H2O / 14 h / Heating View Scheme
参考文献
Mironova; Leont'eva; Shevyakov; Alexeeva; Shvets; Demina; Krasnokutskaya; Finkel'shtein; Khodonov
Russian Journal of Bioorganic Chemistry, 2002 , vol. 28, # 6 p. 487 - 493
反应条件
sodium cyanide; manganese(IV) oxide; acetic acid
T=4 - 20°C;
参考文献
Mironova; Leont'eva; Shevyakov; Alexeeva; Shvets; Demina; Krasnokutskaya; Finkel'shtein; Khodonov
Russian Journal of Bioorganic Chemistry, 2002 , vol. 28, # 6 p. 487 - 493