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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
335343-05-0
合成路线
（共 26 条）
668987-38-0
→
反应条件
335343-05-0
反应条件
[1,3-bis(diphenylphosphino) propane] dichloronickel(II); triphenylphosphine; zinc T=100°C; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
98910-57-7
+
335343-05-0
→
反应条件
4877-93-4
2,2’-二甲氧基联苯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium phosphate; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; 48 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Resmerita, Ana-Maria; Rosen, Brad M.; Percec, Virgil
Journal of Organic Chemistry, 2011 , vol. 76, # 24 p. 9946 - 9955
1137-57-1
+
335343-05-0
→
反应条件
4877-93-4
2,2’-二甲氧基联苯
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 48 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
109384-19-2
N-Boc-4-羟基哌啶
+
335343-05-0
→
反应条件
201609-28-1
4-羟基-4-(2-甲氧基苯基)哌啶-1-羧酸叔丁酯
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; chlorobenzene; cesium fluoride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene T=80°C; 9 h; Inert atmosphere;
参考文献
Berini, Christophe; Navarro, Oscar
Chemical Communications, 2012 , vol. 48, # 10 p. 1538 - 1540
124-38-9
二氧化碳
+
335343-05-0
→
反应条件
579-75-9
邻甲氧基苯甲酸
反应条件
4-MeO-dppp; cesium fluoride; [Rh(OH)(cycloocta-1,5-diene)]2 in 1,4-dioxane T=60°C;
参考文献
Ukai, Kazutoshi; Aoki, Masao; Takaya, Jun; Iwasawa, Nobuharu
Journal of the American Chemical Society, 2006 , vol. 128, # 27 p. 8706 - 8707
1138-66-5
+
335343-05-0
→
反应条件
24423-09-4
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 18 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
52200-03-0
3-甲氧基苯基甲烷磺酸酯
+
335343-05-0
→
反应条件
24423-09-4
反应条件
potassium phosphate; trans-[Ni(Naph)Cl(PPh3)2]; tri-cyclo-hexyl-phosphine in tetrahydrofuran T=25°C; Suzuki coupling; 12 h; Inert atmosphere;
参考文献
Leowanawat, Pawaret; Zhang, Na; Safi, Mehtap; Hoffman, David J.; Fryberger, Miriam C.; George, Aiswaria; Percec, Virgil
Journal of Organic Chemistry, 2012 , vol. 77, # 6 p. 2885 - 2892
273-53-0
苯并恶唑
+
335343-05-0
→
反应条件
13459-17-1
反应条件
oxygen; copper(l) chloride; lithium tert-butylate in N,N-dimethyl-formamide T=40°C; P=760.051 Torr; 0.166667 h;
参考文献
Yang, Fanzhi; Xu, Zhaoqing; Wang, Zhe; Yu, Zhengkun; Wang, Rui
Chemistry - A European Journal, 2011 , vol. 17, # 23 p. 6321 - 6325
335343-05-0
+
108-93-0
环己醇
→
反应条件
79416-02-7
反应条件
bis(1,5-cyclooctadiene)nickel (0); potassium tert-butylate; chlorobenzene; cesium fluoride; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in toluene T=80°C; 9 h; Inert atmosphere;
参考文献
Berini, Christophe; Navarro, Oscar
Chemical Communications, 2012 , vol. 48, # 10 p. 1538 - 1540
104-92-7
4-溴苯甲醚
+
335343-05-0
→
反应条件
49602-47-3
2,4-二甲氧基联苯
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura cross-coupling; 6 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
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