2-(2-氧代-2-苯乙基)-环己酮合成路线 (共 46 条)
反应条件
T=130°C; aza-Darzens reaction; 0.166667 h; Microwave irradiationneat (no solvent);
参考文献
Ma, Li-Jian; Inokuchi, Tsutomu
Chemical Communications, 2010 , vol. 46, # 37 p. 7037 - 7039
反应条件
lithium carbonate; diphenyldisulfane in dimethyl sulfoxide T=40°C; 6 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.
Journal of Organic Chemistry, 1993 , vol. 58, # 10 p. 2678 - 2685
反应条件
lithium carbonate; diphenyldisulfane in dimethyl sulfoxide T=40°C; 6 h; Irradiation;
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.
Journal of Organic Chemistry, 1993 , vol. 58, # 10 p. 2678 - 2685
反应条件
hydrogenchloride; potassium dichromate in water; acetonitrile 16 h; Irradiation;
参考文献
Mitani, Michiharu; Tamada, Mamoru; Uehara, Shin-ichi; Koyama, Kikuhiko
Tetrahedron Letters, 1984 , vol. 25, # 26 p. 2805 - 2808
反应条件
1: 1-(trimethylsilyloxy)-1-cyclohexene With methyllithium in diethyl ether T=0°C; 0.5 h; 2: With gallium(III) chloride in diethyl ether; hexane T=0 - 20°C; 0.5 h; 3: phenacyl iodine With air; triethyl borane in diethyl ether; hexane T=25°C; 0.5 h;
参考文献
Usugi, Shin-ichi; Yorimitsu, Hideki; Shinokubo, Hiroshi; Oshima, Koichiro
Bulletin of the Chemical Society of Japan, 2002 , vol. 75, # 9 p. 2049 - 2052
反应条件
[VO(OEt)Cl2] in dichloromethane 1) -75 deg C, 3 h, 2) -30 deg C, 4 h;
参考文献
Fujii Takashi; Hirao, Toshikazu; Ohshiro, Yoshiki
Tetrahedron Letters, 1992 , vol. 33, # 39 p. 5823 - 5826
反应条件
tetrabutylammonium hexanitratocerate(IV); Ph(CH=CH2)OSi(t-Bu)Me2; potassium carbonate in acetonitrile T=0°C; 2 h;
参考文献
Kohno, Yasushi; Narasaka, Koichi
Bulletin of the Chemical Society of Japan, 1995 , vol. 68, # 1 p. 322 - 329
反应条件
1: 30 percent / Li2CO3 / dimethylsulfoxide / 6 h / 40 °C / Irradiation 2: H2O, HgCl2 / acetonitrile / 6 h / Heating View Scheme
参考文献
Russell, Glen A.; Kulkarni, Shekhar V.; Khanna, Rajive K.
Journal of Organic Chemistry, 1990 , vol. 55, # 3 p. 1080 - 1086
参考文献
Zhdankin, Viktor V.; Tykwinski, Rik; Caple, Roland; Berglund, Bruce; Koz'min, Anatoly S.; Zefirov, Nikolai S.
Tetrahedron Letters, 1988 , vol. 29, # 30 p. 3703 - 3704
反应条件
1: dimethylsulfoxide / 10 h / Irradiation 2: 60 percent / aq. HCl / 0.5 h View Scheme
参考文献
Cranwell, Philippa B.; O'Brien, Matthew; Browne, Duncan L.; Koos, Peter; Polyzos, Anastasios; Pena-Lopez, Miguel; Ley, Steven V.
Organic and Biomolecular Chemistry, 2012 , vol. 10, # 30 p. 5774 - 5779