烯丙基(氯甲基)二甲硅烷合成路线 （共 14 条）
反应条件
3-chloroprop-1-ene in diethyl ether 3 h; Heating;
参考文献
Zhun', V.I.; Tsvetkov, A. L.; Sheludyakov, V. D.; Lavygin, I. A.; Leitan, O. V.; et al.
J. Gen. Chem. USSR (Engl. Transl.), 1988 , vol. 58, # 7 p. 1599 - 1606,1425 - 1431
参考文献
Merrell Pharmaceuticals Inc.
Patent: US5536732 A1, 1996 ;
Title/Abstract Full Text Show Details
Merrell Dow Pharmaceuticals, Inc.
Patent: US5252587 A1, 1993 ;
反应条件
(i) Mg, Et2O, (ii) /BRN= 1731933/; Multistep reaction;
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 41, p. 1277 - 1279,1286 - 1288
参考文献
Journal of Physical Organic Chemistry, , vol. 23, # 9 p. 859 - 865
参考文献
Doklady Chemistry, , vol. 147, p. 967 - 968
Doklady Akademii Nauk SSSR, , vol. 147, p. 117 - 118
反应条件
hydrogen sulfide T=70 - 80°C; 9 h; Irradiation;
参考文献
Voronkov, M. G.; Kirpichenko, S. V.; Suslova, E. N.; Keiko, V. V.; Albanov, A. I.
Journal of Organometallic Chemistry, 1983 , vol. 243, # 3 p. 271 - 280
参考文献
J. Gen. Chem. USSR (Engl. Transl.), , vol. 53, # 11 p. 2456 - 2464,2215 - 2222
反应条件
ethylaluminum dichloride 1.) CH2Cl2, hexanes, r.t., 30 min, 2. ether, reflux, 3 h; Yield given. Multistep reaction. Title compound not separated from byproducts;
参考文献
Journal of Organic Chemistry, , vol. 57, # 24 p. 6552 - 6556
反应条件
ethyl bromide; magnesium 1.) ether, RT, 2 h, 2.) ether, reflux, 4 h; Yield given. Multistep reaction;
参考文献
Saigo, Kazuhide; Tateishi, Kazuo; Adachi, Hiroshi; Saotome, Yasushi
Journal of Organic Chemistry, 1988 , vol. 53, # 7 p. 1572 - 1574
反应条件
boron trifluoride in dichloromethane
T=20°C; 24 h;
参考文献
Mayr, Herbert; Gorath, Gorden
Journal of the American Chemical Society, 1995 , vol. 117, # 30 p. 7862 - 7867
