3-(2-羟乙基)-2-恶唑烷酮合成路线 (共 15 条)
反应条件
selenium; oxygen; acetonitrile
参考文献
Phosphorus and Sulfur and the Related Elements, , vol. 38, p. 137 - 148
反应条件
hydrogen; palladium dihydroxide in methanol T=20°C; 2 h;
参考文献
EP1721905 A1, ;
Page/Page column 31 ;
反应条件
in ethylene glycol T=98 - 103°C; 12.5 h; Conversion of starting material;
参考文献
US2005/27120 A1, ;
Page/Page column 12 ;
参考文献
WO2010/103281 A1, ;
Page/Page column 18 ;
反应条件
nanoparticulated CeO2 in ethanol T=160°C; P=5250.53 Torr; 8 h; Sealed reactor;
参考文献
Chemical Communications, , vol. 46, # 23 p. 4181 - 4183
反应条件
potassium hydroxide in toluene 15 h; Ambient temperature;
参考文献
Journal of Medicinal Chemistry, , vol. 39, # 10 p. 1991 - 2007
反应条件
1,3-bis(tert-butyl)-imidazolium-2-carboxylate in isopropyl alcohol T=90°C; P=37503.8 Torr; 20 h; Inert atmosphereAutoclave;
参考文献
Green Chemistry, , vol. 15, # 2 p. 425 - 430
反应条件
sodium hydroxide; potassium dihydrogenphosphate; water pH 7,4 ; 5 deg C, 30 min, then room t., 3 h;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2509 - 2515
反应条件
1: 52 percent / NaNO2, HCOOH / 2 h / 5 °C 2: 86 percent / 6.8 g KH2PO4, 1.6 g NaOH, 50 ml water / pH 7,4 ; 5 deg C, 30 min, then room t., 3 h View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 29, # 9 p. 2509 - 2515
参考文献
Journal of Organic Chemistry, , vol. 26, p. 3495 - 3498