N-(2-羟基-2-甲基丙基)苯甲酰胺合成路线 (共 17 条)
反应条件
water Ring cleavage; hydrolysis; 72 h;
参考文献
Besbes, Neji
Tetrahedron Letters, 1999 , vol. 40, # 36 p. 6569 - 6570
反应条件
(4)-MeOC6H4-CHNa-CN in tetrahydrofuran 144 h;
参考文献
Assithianakis, Petros; Stamm, Helmut
Chemische Berichte, 1987 , vol. 120, p. 855 - 858
反应条件
C6H5(C2H5)CNa-CN in tetrahydrofuran 192 h;
参考文献
Assithianakis, Petros; Stamm, Helmut
Chemische Berichte, 1987 , vol. 120, p. 855 - 858
反应条件
silica gel in diethyl ether T=20°C; 72 h;
参考文献
Besbes, Neji; Jellali, Houyem; Pale, Patrick; Efrit, Mohamed Lotfi; Srasra, Ezzeddine
Phosphorus, Sulfur and Silicon and the Related Elements, 2010 , vol. 185, # 4 p. 883 - 889
参考文献
Sheehan; Laubach
Journal of the American Chemical Society, 1951 , vol. 73, p. 4376,4379
反应条件
Xanthenyllithium in tetrahydrofuran 192 h; Ambient temperature;
参考文献
Stamm, Helmut; Sommer, Andreas; Woderer, Anton; Wiesert, Wolfgang; Mall, Thomas; Assithianakis, Petros
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4946 - 4955
反应条件
1: anthracene With sodium in tetrahydrofuran T=20°C; Metallation; 2: N-benzoyl-2,2-dimethylaziridine in tetrahydrofuran T=20°C; Ring cleavage; addition; reduction; 48 h; Further byproducts given. Title compound not separated from byproducts;
参考文献
Lin, Pen-Yuan; Weiss, Rainer; Werry, Juergen; Falkenstein, Reinhard; Stamm, Helmut
Journal fuer Praktische Chemie - Practical Applications and Applied Chemistry (Germany), 2000 , vol. 342, # 2 p. 153 - 161
反应条件
sodium in tetrahydrofuran 72 h; Ambient temperature; Further byproducts given;
参考文献
Lin, Pen-Yuan; Bellos, Konstantinos; Werry, Juergen; Assithianakis, Petros; Weiss, Rainer; Mall, Thomas; Bentz, Gunther; Stamm, Helmut
Journal fur Praktische Chemie - Chemiker - Zeitung, 1996 , vol. 338, # 3 p. 270 - 278
反应条件
indolyllithium in tetrahydrofuran 168 h; Ambient temperature; Title compound not separated from byproducts;
参考文献
Onistschenko, Andreas; Stamm, Helmut
Chemische Berichte, 1989 , vol. 122, p. 2397 - 2398
反应条件
n-butyllithium 1.) THF, from -65 deg C to RT, 2.) THF, RT, 8 d; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Stamm, Helmut; Sommer, Andreas; Woderer, Anton; Wiesert, Wolfgang; Mall, Thomas; Assithianakis, Petros
Journal of Organic Chemistry, 1985 , vol. 50, # 24 p. 4946 - 4955