3-碘喹啉-2(1h)-酮合成路线 （共 7 条）
反应条件
potassium carbonate; benzoyl chloride in dichloromethane; water T=0 - 20°C;
参考文献
Boganyi, Borbala; Kaman, Judit
Tetrahedron, 2013 , vol. 69, # 45 p. 9512 - 9519
反应条件
in water; acetic acid
参考文献
Fraley, Mark E.; Karki, Shyam B.; Kim, Yuntae
Patent: US2002/72526 A1, 2002 ;
反应条件
1: m-chloroperbenzoic acid / CH2Cl2 / 17 h / 20 °C 2: benzoyl chloride; sodium hydroxide / CH2Cl2; H2O / 1 h View Scheme
参考文献
Boganyi, Borbala; Kaman, Judit
Tetrahedron, 2013 , vol. 69, # 45 p. 9512 - 9519
反应条件
1.1: HBF4; isoamyl nitrite / acetone / 1 h / -8 - 10 °C 1.2: 86 percent / KI / acetone; H2O / 2 h 2.1: m-chloroperbenzoic acid / CH2Cl2 / 17 h / 20 °C 3.1: benzoyl chloride; sodium hydroxide / CH2Cl2; H2O / 1 h View Scheme
参考文献
Loones, Kristof T.J.; Maes, Bert U.W.; Dommisse, Roger A.
Tetrahedron, 2007 , vol. 63, # 36 p. 8954 - 8961
反应条件
1: sodium iodide; N,N-dimethylethylenediamine; copper(l) iodide / 1,4-dioxane / 8 h / 100 °C / |Inert atmosphere 2: 3-chloro-benzenecarboperoxoic acid / dichloromethane / 20 °C 3: benzoyl chloride; potassium carbonate / dichloromethane; water / 0 - 20 °C View Scheme
参考文献
Boganyi, Borbala; Kaman, Judit
Tetrahedron, 2013 , vol. 69, # 45 p. 9512 - 9519
反应条件
trichlorophosphate in toluene 2 h; Heating;
参考文献
Loones, Kristof T.J.; Maes, Bert U.W.; Dommisse, Roger A.
Tetrahedron, 2007 , vol. 63, # 36 p. 8954 - 8961
反应条件
1: phosphorus oxytribromide / toluene / 3 h / 0 °C / |Reflux
2: palladium diacetate; 9,9-dimethyl-4,5-bis(diphenyl-phosphino)xanthene; caesium carbonate / toluene / 1.5 h / 120 °C / |Inert atmosphere; |Microwave irradiation
3: bis-triphenylphosphine-palladium(II) chloride; sodium acetate / N,N-dimethyl acetamide / 1 h / 150 °C / |Inert atmosphere; |Microwave irradiation
View Scheme
参考文献
Boganyi, Borbala; Kaman, Judit
Tetrahedron, 2013 , vol. 69, # 45 p. 9512 - 9519
