(3E,5Z)-辛-1,3,5-三烯合成路线 (共 24 条)
反应条件
1: 85 percent 2: sat. thiourea, NaHCO3 / H2O / 4 h / Ambient temperature 3: 85 percent / Ph3P / diethyl ether / 0.25 h / Ambient temperature View Scheme
参考文献
Goldbach, Michael; Jaekel, Edgar; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1987 , # 19 p. 1434 - 1435
反应条件
1: sat. thiourea, NaHCO3 / H2O / 4 h / Ambient temperature 2: 85 percent / Ph3P / diethyl ether / 0.25 h / Ambient temperature View Scheme
参考文献
Goldbach, Michael; Jaekel, Edgar; Schneider, Manfred P.
Journal of the Chemical Society, Chemical Communications, 1987 , # 19 p. 1434 - 1435
反应条件
1: KOtBu 2: MeLi 3: 270 °C View Scheme
参考文献
Minter,D.E.; Fonken,G.J.
Tetrahedron Letters, 1977 , p. 4149 - 4152
参考文献
Schneider; Goldbach
Journal of the American Chemical Society, 1980 , vol. 102, # 19 p. 6114 - 6116