1-甲烷磺酰基-4-苯乙炔苯合成路线 (共 4 条)
反应条件
Oxonereg; in tetrahydrofuran; methanol; water T=25°C; 1.5 h;
参考文献
Chen, Qiao-Hong; Rao, P. N. Praveen; Knaus, Edward E.
Bioorganic and Medicinal Chemistry, 2005 , vol. 13, # 23 p. 6425 - 6434
反应条件
1: 47 percent / copper(I) iodide; triethylamine / dichlorobis(triphenylphosphine)palladium / 90 °C 2: 83 percent / Oxone(R) / H2O; methanol; tetrahydrofuran / 1.5 h / 25 °C View Scheme
参考文献
Friesen, Richard W.; Dube, Daniel; Fortin, Rejean; Frenette, Richard; Prescott, Sylvie; Cromlish, Wanda; Greig, Gillian M.; Kargman, Stacia; Wong, Elizabeth; Chan, Chi Chung; Gordon, Robert; Xu, Li Jing; Riendeau, Denis
Bioorganic and Medicinal Chemistry Letters, 1996 , vol. 6, # 22 p. 2677 - 2682
参考文献
Eisch,J.J.; Hordis,C.K.
Journal of the American Chemical Society, 1971 , vol. 93, # 12 p. 2974 - 2981
反应条件
formic acid; methanesulfonic acid; dimethyl sulfoxide; hydrogen bromide
T=105 - 110°C; 15 h;
参考文献
Wan, Zhonghui; Jones, Chauncey D.; Mitchell, David; Pu, John Y.; Zhang, Tony Y.
Journal of Organic Chemistry, 2006 , vol. 71, # 2 p. 826 - 828