(1-溴甲基-乙烯基)-苯合成路线 （共 50 条）
反应条件
toluene-4-sulfonic acid
参考文献
Ravindranath, B.; Srinivas, P.
Indian Journal of Chemistry, Section B: Organic Chemistry Including Medicinal Chemistry, 1983 , vol. 22, # 6 p. 592 - 594
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in tetrachloromethane T=95°C; D-labelled; Mechanism;
参考文献
Mulzer, Johann; Bruentrup, Gisela; Kuehl, Uwe; Hartz, Georg
Chemische Berichte, 1982 , vol. 115, # 11 p. 3453 - 3469
反应条件
(tBuOOCO)2; hydrogen bromide; oxygen in tetrahydrofuran; hexane T=30°C; 1 h; pH=2-4; Product distribution;
参考文献
Jiang, Xi-Kui; Liu, Wayne Wei-Zhong; Wu, Shi-Hui
Journal of Physical Organic Chemistry, 1994 , vol. 7, p. 96 - 104
反应条件
bromine; dibenzoyl peroxide in tetrachloromethane Heatingother substituted arenes; var. reagents and time; Product distribution;
参考文献
Sket, Boris; Zupan, Marko
Journal of Organic Chemistry, 1986 , vol. 51, # 6 p. 929 - 931
反应条件
T=350°C; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Jiang, Xi-Kui; Liu, Wayne Wei-Zhong; Wu, Shi-Hui
Journal of Physical Organic Chemistry, 1994 , vol. 7, p. 96 - 104
反应条件
1: 1H-benzo[d]imidazole With sodium hydride in tetrahydrofuran; mineral oil 0.25 h; Cooling with iceInert atmosphere; 2: 1-bromo-2-phenyl-2-propene in tetrahydrofuran; mineral oil T=20°C; 18 h; Inert atmosphere;
参考文献
Tsai, Andy S.; Wilson, Rebecca M.; Harada, Hitoshi; Bergman, Robert G.; Ellman, Jonathan A.
Chemical Communications, 2009 , # 26 p. 3910 - 3912
反应条件
di-tert-butyl peroxide; potassium carbonate T=120°C; 93 h;
参考文献
Struss, John A.; Sadeghipour, Mitra; Tanko, James M.
Tetrahedron Letters, 2009 , vol. 50, # 18 p. 2119 - 2120
反应条件
sodium carbonate; potassium iodide in N,N-dimethyl-formamide 22.5 h; Ambient temperature;
参考文献
Kukla, Michael J.; Breslin, Henry J.; Pauwels, Rudi; Fedde, Cynthia L.; Miranda, Milton; et al.
Journal of Medicinal Chemistry, 1991 , vol. 34, # 2 p. 746 - 751
反应条件
1: 75 percent / sodium hydride / tetrahydrofuran / 4 h / 20 °C 2: RuCl2(PCy3)(benzylidene)(1,3-dimesitylimidazol-2-ylidene) / CH2Cl2 / 6 h / Heating View Scheme
参考文献
Bujard; Briot; Gouverneur; Mioskowski
Tetrahedron Letters, 1999 , vol. 40, # 50 p. 8785 - 8788
反应条件
1: 62 percent / 85percent H2O2, 1,3-dibromo-5,5-dimethylhydanthoin (DDH) / diethyl ether; H2O / 2 h / 0 °C 2: 48 percent / NaOH / CH2Cl2; H2O / 2 h / 0 °C 3: tetrahydrofuran; hexane / 1 h / -78 °C View Scheme
参考文献
Adam, Waldemar; Heil, Markus
Chemische Berichte, 1992 , vol. 125, # 1 p. 235 - 241
