4-甲氧基-n-甲基-2-硝基苯胺合成路线 (共 18 条)
反应条件
silver nitrate 15 h; Ambient temperature;
参考文献
Baum, Marc M.; Smith, Edward H.
Journal of the Chemical Society, Chemical Communications, 1991 , # 6 p. 431 - 432
反应条件
sulfuric acid; acetic acid
参考文献
Takeda Kenkyusho Nenpo, , vol. 8, p. 22,24,26
Chem.Abstr., , p. 4854
反应条件
1: water; acetic acid; nitric acid 2: diluted aq. NaOH solution 3: acetic acid; concentrated sulfuric acid View Scheme
参考文献
Takeda Kenkyusho Nenpo, , vol. 8, p. 22,24,26
Chem.Abstr., , p. 4854
反应条件
1: diluted aq. NaOH solution 2: acetic acid; concentrated sulfuric acid View Scheme
参考文献
Takeda Kenkyusho Nenpo, , vol. 8, p. 22,24,26
Chem.Abstr., , p. 4854
反应条件
piperidine in benzene T=100°C; other substituted N-methyl-N-nitroanilines; ΔH(excit.), ΔS(excit.); effect of pressure; mechanism; var. solvents; Rate constantThermodynamic dataProduct distribution;
参考文献
Journal of the Chemical Society. Perkin Transactions 2, , vol. 7, p. 1321 - 1324
反应条件
1: tin; aqueous HCl / Erhitzen des Reaktionsprodukts mit wss. Ameisensaeure 2: xylene; NaNH2 View Scheme
参考文献
Simonow; Uglow
Zhurnal Obshchei Khimii, 1951 , vol. 21, p. 884,886; engl. Ausg. S. 971, 973
反应条件
hydrogenchloride; Pd-C in ethanol
参考文献
A/S Ferrosan
Patent: US4948794 A1, 1990 ;
反应条件
1: Et3N / benzene
2: aq. NaOH
View Scheme
参考文献
Bianchi,M. et al.
European Journal of Medicinal Chemistry, 1976 , vol. 11, p. 101 - 106