(2Z)-3-氯-3-苯基-2-丙烯醛合成路线 （共 23 条）
反应条件
1,4-diaza-bicyclo[2.2.2]octane; AlCl3, aluminium chloride T=20°C; Baylis-Hillman reaction; 24 h; Neat (no solvent);
参考文献
Zhong, Weihui; Chen, Yanhui; Wang, Guan
Journal of Chemical Research, 2010 , # 1 p. 44 - 49
反应条件
1,4-diaza-bicyclo[2.2.2]octane; AlCl3, aluminium chloride T=20°C; Baylis-Hillman reaction; 72 h; Neat (no solvent)Sonication;
参考文献
Zhong, Weihui; Chen, Yanhui; Wang, Guan
Journal of Chemical Research, 2010 , # 1 p. 44 - 49
反应条件
1,4-diaza-bicyclo[2.2.2]octane T=50°C; Baylis-Hillman reaction; 3.5 h; Neat (no solvent)Sonication;
参考文献
Zhong, Weihui; Jiang, Lingbo; Guo, Baoming; Wu, Yaotiao; Hong, Lingjuan; Chen, Yanhui
Synthetic Communications, 2010 , vol. 40, # 16 p. 2441 - 2456
反应条件
1,4-diaza-bicyclo[2.2.2]octane; AlCl3, aluminium chloride T=20°C; Baylis-Hillman reaction; 72 h; Neat (no solvent);
参考文献
Zhong, Weihui; Chen, Yanhui; Wang, Guan
Journal of Chemical Research, 2010 , # 1 p. 44 - 49
反应条件
1,4-diaza-bicyclo[2.2.2]octane T=50°C; Baylis-Hillman reaction; 3.5 h; Neat (no solvent)Sonication;
参考文献
Zhong, Weihui; Jiang, Lingbo; Guo, Baoming; Wu, Yaotiao; Hong, Lingjuan; Chen, Yanhui
Synthetic Communications, 2010 , vol. 40, # 16 p. 2441 - 2456
反应条件
Ammonium thiocyanate in acetone
Heating;
参考文献
Pavlik, James W.; Tongcharoensirikul, Pakamas; Bird, Nigel P.; Day, A. Colin; Barltrop, John A.
Journal of the American Chemical Society, 1994 , vol. 116, # 6 p. 2292 - 2300
反应条件
sodium azide in dimethyl sulfoxide
T=10 - 30°C; 0.333333 h;
参考文献
Brahma, Sulagna; Ray, Jayanta K.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6575 - 6578
反应条件
1,8-diazabicyclo[5.4.0]undec-7-ene; 1,3-bis(2,6-diisopropylphenyl)imidazolinium chloride in tetrahydrofuran
T=-20°C; 5 h; Inert atmosphere;
参考文献
Yao, Weijun; Bian, Ming; Wang, Gang; Ma, Cheng
Synthesis, 2011 , # 12 art. no. C28111SS, p. 1998 - 2002
反应条件
diethylamine in tetrahydrofuran
1 h; Heating;
参考文献
Joseph, Delphine; Jankowski, Raphael; Prim, Damien; Mahuteau, Jacqueline; Chiaroni, Angele
Tetrahedron Letters, 2002 , vol. 43, # 45 p. 8051 - 8054
反应条件
sodium azide in dimethyl sulfoxide
T=10 - 30°C; 0.333333 h;
参考文献
Brahma, Sulagna; Ray, Jayanta K.
Tetrahedron Letters, 2005 , vol. 46, # 38 p. 6575 - 6578
