2-(10-溴癸基)-5,6-二甲氧基-3-甲基-1,4-苯二酚合成路线 （共 4 条）
反应条件
sodium dithionite; water in ethyl acetate Inert atmosphere;
参考文献
Ma, Wei; Li, Da-Wei; Sutherland, Todd C.; Li, Yang; Long, Yi-Tao; Chen, Hong-Yuan
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12366 - 12369
反应条件
1: thionyl chloride / 0.25 h / 90 °C 2: dihydrogen peroxide / pyridine; diethyl ether / 1.75 h / 0 - 20 °C 3: acetic acid / 20 h / 100 °C 4: potassium borohydride / methanol / 0.5 h / 0 °C View Scheme
参考文献
Ma, Wei; Li, Da-Wei; Sutherland, Todd C.; Li, Yang; Long, Yi-Tao; Chen, Hong-Yuan
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12366 - 12369
反应条件
1: dihydrogen peroxide / pyridine; diethyl ether / 1.75 h / 0 - 20 °C 2: acetic acid / 20 h / 100 °C 3: potassium borohydride / methanol / 0.5 h / 0 °C View Scheme
参考文献
Ma, Wei; Li, Da-Wei; Sutherland, Todd C.; Li, Yang; Long, Yi-Tao; Chen, Hong-Yuan
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12366 - 12369
反应条件
1: acetic acid / 20 h / 100 °C 2: potassium borohydride / methanol / 0.5 h / 0 °C View Scheme
参考文献
Ma, Wei; Li, Da-Wei; Sutherland, Todd C.; Li, Yang; Long, Yi-Tao; Chen, Hong-Yuan
Journal of the American Chemical Society, 2011 , vol. 133, # 32 p. 12366 - 12369
