(2R,6S)-6-甲氧基-2-甲基-6H-吡喃-3-酮合成路线 （共 2 条）
反应条件
1: NaBH4 2: 2.) N-iodosuccinimide 3: 1.) tributyltin hydride, 2.) 5M aq. NaOH View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
反应条件
1: 7 percent / sodium borohydride / tetrahydrofuran; H2O / 0.5 h / 0 °C 2: 1.) sodium hydride / 1.) THF, 0 deg C, 1 h, 2.) THF, 0 deg C, 2 h 3: 71 percent / NIS / CHCl3 / 12 h / Ambient temperature 4: 78 percent / Bu3SnH / AIBN / benzene / 3 h / Heating 5: 72 percent / PTSA, pyridine / H2O / 2 h / 100 °C View Scheme
参考文献
Sammes, Peter G.; Thetford, Dean
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1988 , p. 111 - 124
