2,4,6-三甲基二苯硫醚合成路线 (共 20 条)
反应条件
1,10-phenanthroline; oxygen; anhydrous copper acetate in dimethyl sulfoxide T=100°C; 2 h; Air atmosphere;
参考文献
Yasuike, Shuji; Nishioka, Motokazu; Kakusawa, Naoki; Kurita, Jyoji
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6403 - 6406
反应条件
copper(l) iodide; 2,9-dimethyl-1,10-phenanthroline; sodium t-butanolate in toluene T=110°C; 24 h;
参考文献
Bates, Craig G; Gujadhur, Rattan K; Venkataraman
Organic letters, 2002 , vol. 4, # 16 p. 2803 - 2806
反应条件
1,10-phenanthroline; oxygen; anhydrous copper acetate in dimethyl sulfoxide T=100°C; 2 h; Air atmosphere;
参考文献
Yasuike, Shuji; Nishioka, Motokazu; Kakusawa, Naoki; Kurita, Jyoji
Tetrahedron Letters, 2011 , vol. 52, # 48 p. 6403 - 6406
反应条件
Pd(2-[2-(benzylthio)phenyliminomethyl]-4-bromophenol-(H))Cl; potassium carbonate in N,N-dimethyl-formamide T=90°C; 5 h; Sealed tubeInert atmosphere;
参考文献
Gogoi, Prasanta; Kalita, Mukul; Barman, Pranjit
Synlett, 2014 , vol. 25, # 6 art. no. 47, p. 866 - 870
反应条件
[Pd(1,3-bis(2,6-bis(diphenylmethyl)-4-methylphenyl)imidazol-2-ylidene)(cinnamyl)Cl]; potassium tert-butylate in 1,4-dioxane T=110°C; 12 h; GloveboxInert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9303 - 9308
反应条件
palladium diacetate in trifluoroacetic acid T=20°C; 6 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
dipotassium peroxodisulfate in trifluoroacetic acid T=20°C; 8 h;
参考文献
Prasad, Ch Durga; Balkrishna, Shah Jaimin; Kumar, Amit; Bhakuni, Bhagat Singh; Shrimali, Kaustubh; Biswas, Soumava; Kumar, Sangit
Journal of Organic Chemistry, 2013 , vol. 78, # 4 p. 1434 - 1443
反应条件
palladium diacetate; trifluoroacetic acid T=20°C; 0.75 h; SolventTimeReagent/catalystConcentration;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851
反应条件
[Pd(1,3-bis(2,6-bis(diphenylmethyl)-4-methylphenyl)imidazol-2-ylidene)(cinnamyl)Cl]; potassium tert-butylate in 1,4-dioxane T=110°C; 12 h; GloveboxInert atmosphere;
参考文献
Bastug, Gulluzar; Nolan, Steven P.
Journal of Organic Chemistry, 2013 , vol. 78, # 18 p. 9303 - 9308
反应条件
palladium diacetate in trifluoroacetic acid T=20°C; 24 h;
参考文献
Saravanan, Perumal; Anbarasan, Pazhamalai
Organic Letters, 2014 , vol. 16, # 3 p. 848 - 851