2,4,6-三甲基二苯硫醚合成路线 (共 20 条)
反应条件
tin(IV) chloride in various solvent(s) 1 h; Ambient temperature;
参考文献
Bottino, Francesco; Fradullo, Rosa; Pappalardo, Sebastiano
Journal of Organic Chemistry, 1981 , vol. 46, # 13 p. 2793 - 2795
反应条件
sodium hydroxide; 2,4,6-trimethylphenyl diazonium chloride
参考文献
Gazzetta Chimica Italiana, , vol. 84, p. 3,20
反应条件
in dimethyl sulfoxide T=25°C; 5.5 h;
参考文献
Petrillo, Giovanni; Novi, Marino; Garbarino, Giacomo; Dell'Erba, Carlo
Tetrahedron Letters, 1985 , vol. 26, # 51 p. 6365 - 6368
反应条件
isopentyl nitrite in 1,4-dioxane; 1,2-dichloro-ethane 0.75 h; Heating;
参考文献
Nakayama, Juzo; Fujita, Toko; Hoshino, Masamatsu
Chemistry Letters, 1983 , p. 249 - 250
反应条件
1: Benzenesulfonyl cyanide With palladium diacetate; trifluoroacetic acid T=20°C; 0.166667 h; 2: 1,3,5-trimethyl-benzene T=20°C; 1 h;
参考文献
Anbarasan, Pazhamalai; Neumann, Helfried; Beller, Matthias
Chemical Communications, 2011 , vol. 47, # 11 p. 3233 - 3235
反应条件
sodium hydroxide; benzene diazonium chloride
参考文献
Gazzetta Chimica Italiana, , vol. 84, p. 3,20
反应条件
1.1: sulfuryl dichloride; triethylamine / dichloromethane / 0 - 20 °C 1.2: 1 h / 0 - 20 °C 2.1: palladium diacetate / trifluoroacetic acid / 6 h / 20 °C View Scheme
参考文献
Organic Letters, , vol. 16, # 3 p. 848 - 851
反应条件
tetrakis(triphenylphosphine) palladium(0) in toluene T=120°C; 20 h;
参考文献
Kosugi, Masanori; Ogata, Toshimi; Terada, Masahiro; Sano, Hiroshi; Migita, Toshihiko
Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 12 p. 3657 - 3658
参考文献
Chemische Berichte, , vol. 28, p. 2319
Recueil des Travaux Chimiques des Pays-Bas, , vol. 18, p. 433
反应条件
dihydrogen peroxide; acetic acid
参考文献
Leandri et al.
Gazzetta Chimica Italiana, 1954 , vol. 84, p. 73,82