反应条件
1.1: potassium phosphate; CuSO4‵5H2O; 1,10-phenanthroline / toluene / 48 h / Inert atmosphere; Reflux
2.1: N,N,N',N,-tetramethylethylenediamine; sec.-butyllithium / tetrahydrofuran; cyclohexane / 1 h / -78 °C / Inert atmosphere
2.2: -78 - 20 °C / Inert atmosphere
View Scheme
参考文献
Gati, Wafa; Rammah, Mohamed M.; Rammah, Mohamed B.; Evano, Gwilherm
Beilstein Journal of Organic Chemistry, 2012 , vol. 8, p. 2214 - 2222